VAMAS Surface Chemical Analysis Standard Data Transfer Format 1988 May 4 Not Specified Not Specified Not Specified Not Specified 7 Casa Info Follows 0 SourceAnalyserAngle: Not Specified CasaRowLabel:nb_sba10.vms CasaRowLabel:nb_sba2.vms CasaRowLabel:nb_sba5.vms CasaRowLabel:pnb.vms MAP REGULAR 6 0 0 0 1 Data Set d 0 0 0 0 21 wide/1 nb_sba10.vms 2015 12 10 7 0 32 0 9 Casa Info Follows 0 0 0 0 nb_sba10.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 160 Acqn. Time(s): 603 Sweeps: 5 Anode:Mono(Al (Mono))(156 W) Step(meV): 1000.0 Dwell Time(ms): 100 Charge Neutraliser :On Acquired On :15/12/10 07:00:32 XPS 63 7 0 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 160 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Wide None -1 Kinetic Energy eV 286.69 1 2 Intensity d Transmission d pulse counting 0.1 5 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 2412 6 23205 4.41569 8.42235 3431 8.42235 3438 8.38839 3522 8.35442 3508 8.32045 3454 8.28649 3462 8.25252 3423 8.21856 3485 8.18459 3410 8.15063 3597 8.11666 3552 8.0827 3555 8.04873 3541 8.01476 3503 7.9808 3592 7.94683 3579 7.91287 3565 7.8789 3523 7.84494 3609 7.81097 3577 7.77701 3596 7.74304 3527 7.70907 3532 7.67511 3589 7.64114 3487 7.60718 3494 7.57321 3664 7.53925 3518 7.50528 3598 7.47131 3543 7.43735 3618 7.40338 3545 7.36942 3504 7.33545 3430 7.30149 3578 7.26752 3549 7.23356 3565 7.19959 3547 7.16562 3578 7.13166 3614 7.09769 3531 7.06373 3627 7.02976 3600 7.00512 3555 6.99202 3684 6.97893 3655 6.96583 3656 6.95273 3645 6.93963 3649 6.92653 3612 6.91343 3578 6.90033 3656 6.88723 3720 6.87414 3708 6.86104 3672 6.84794 3544 6.83484 3613 6.82174 3626 6.80864 3780 6.79554 3666 6.78244 3691 6.76935 3690 6.75625 3774 6.74315 3727 6.73005 3707 6.71695 3659 6.70385 3742 6.69075 3764 6.67765 3662 6.66456 3683 6.65146 3818 6.63836 3768 6.62526 3737 6.61216 3700 6.59906 3893 6.58596 3796 6.57286 3655 6.55976 3761 6.54667 3787 6.53357 3788 6.52047 3784 6.50737 3828 6.49427 3828 6.48117 3880 6.46807 3989 6.45497 3850 6.44188 3909 6.42878 3912 6.41568 3717 6.40258 3903 6.38948 3945 6.37638 3797 6.36328 3792 6.35018 3785 6.33709 3817 6.32399 3818 6.31089 3913 6.29779 3812 6.28469 3853 6.27159 3925 6.25849 3941 6.24539 3882 6.2323 3976 6.2192 3846 6.2061 3964 6.193 3969 6.1799 4010 6.1668 3894 6.1537 3923 6.1406 3941 6.1275 4002 6.11441 4025 6.10131 4079 6.08821 3928 6.07511 4151 6.06201 3991 6.04891 3981 6.03581 3885 6.02271 3934 6.00962 4018 5.99652 4057 5.98342 3981 5.97032 4013 5.95722 3989 5.94412 4083 5.93102 3989 5.91792 4002 5.90483 3962 5.89173 4087 5.87863 4033 5.86553 4175 5.85243 4256 5.83933 4072 5.82623 4297 5.81313 4059 5.80004 4130 5.78694 4116 5.77384 4137 5.76074 4174 5.74764 4231 5.73454 4228 5.72144 4214 5.70834 4168 5.69524 4230 5.68215 4245 5.66905 4302 5.65595 4197 5.64285 4267 5.62975 4214 5.61665 4303 5.60355 4294 5.59045 4232 5.57736 4284 5.56426 4331 5.55116 4275 5.53806 4287 5.52496 4302 5.51186 4374 5.49876 4470 5.48566 4463 5.47257 4468 5.45947 4391 5.44637 4425 5.43327 4498 5.42017 4414 5.40707 4422 5.39397 4515 5.38087 4489 5.36778 4472 5.35468 4467 5.34158 4557 5.33457 4519 5.33071 4479 5.32684 4497 5.32297 4433 5.31911 4662 5.31524 4632 5.31137 4633 5.30751 4666 5.30364 4736 5.29978 4688 5.29591 4854 5.29204 4811 5.28818 4731 5.28431 4862 5.28044 4765 5.27658 4874 5.27271 4963 5.26885 4830 5.26498 4826 5.26111 4711 5.25725 4826 5.25338 4890 5.24951 4868 5.24565 4810 5.24178 4940 5.23792 4928 5.23405 5019 5.23018 4999 5.22632 5060 5.22245 5193 5.21858 5332 5.21472 5282 5.21085 5291 5.20699 5155 5.20312 5074 5.19925 5097 5.19539 4969 5.19152 5061 5.18765 4965 5.18379 4766 5.17992 4651 5.17606 4532 5.17219 4661 5.16832 4675 5.16446 4765 5.16059 4655 5.15672 4795 5.15286 5064 5.14899 5448 5.14513 5588 5.14126 5887 5.13739 6205 5.13353 6620 5.12966 6534 5.12579 6281 5.12193 6021 5.11806 5577 5.1142 5156 5.11033 4859 5.10646 4447 5.1026 4189 5.09873 4044 5.09486 3747 5.091 3562 5.08713 3402 5.08327 3221 5.0794 3062 5.07553 2958 5.07167 2925 5.0678 2859 5.06393 2961 5.06007 2953 5.0562 3001 5.05234 2927 5.04847 2995 5.0446 2992 5.04074 3001 5.03687 2904 5.033 2955 5.02914 2966 5.02527 2924 5.02141 3003 5.01754 2986 5.01367 2919 5.00981 2959 5.00594 2969 5.00207 2946 4.99821 2999 4.99434 3091 4.99048 3057 4.98661 3039 4.98274 3025 4.97888 3021 4.97501 3032 4.97114 3165 4.96728 3059 4.96341 2998 4.95955 3000 4.95568 3046 4.95181 2982 4.94795 3047 4.94408 3121 4.94021 3169 4.93635 3002 4.93248 3087 4.92862 3055 4.92475 3056 4.92088 3080 4.91702 3094 4.91315 3072 4.90928 3097 4.90542 3163 4.90155 3127 4.89769 3089 4.89382 3163 4.88995 3196 4.88609 3148 4.88222 3205 4.87835 3156 4.87449 3148 4.87062 3246 4.86676 3183 4.86289 3248 4.85902 3238 4.85516 3238 4.85129 3214 4.84742 3185 4.84356 3281 4.83969 3294 4.83582 3223 4.83196 3173 4.82809 3180 4.82423 3362 4.82036 3338 4.81649 3252 4.81263 3306 4.80876 3146 4.80489 3264 4.80103 3325 4.79716 3316 4.7933 3302 4.78943 3275 4.78556 3261 4.7817 3292 4.77783 3309 4.77396 3320 4.7701 3373 4.76623 3365 4.76237 3329 4.7585 3407 4.75463 3382 4.75077 3450 4.7469 3465 4.74303 3338 4.73917 3436 4.7353 3392 4.73144 3396 4.72757 3529 4.7237 3686 4.71984 3548 4.71597 3413 4.7121 3310 4.70824 3278 4.70437 3288 4.70051 3291 4.69664 3262 4.69277 3421 4.68891 3394 4.68504 3435 4.68117 3554 4.67731 3708 4.67344 3621 4.66958 3512 4.66571 3535 4.66184 3669 4.65798 3744 4.65411 3967 4.65024 3772 4.64638 3637 4.64251 3297 4.63865 3280 4.63478 3285 4.63091 3252 4.62705 3242 4.62318 3272 4.61931 3260 4.61545 3260 4.61158 3224 4.60772 3269 4.60385 3303 4.59998 3352 4.59612 3290 4.59225 3265 4.58838 3300 4.58452 3298 4.58065 3198 4.57679 3316 4.57292 3346 4.56905 3379 4.56519 3363 4.56132 3342 4.55745 3363 4.55359 3403 4.54972 3389 4.54586 3384 4.54199 3358 4.53812 3353 4.53426 3424 4.53039 3365 4.52906 3432 4.52854 3393 4.52803 3349 4.52752 3366 4.52701 3365 4.52649 3437 4.52598 3484 4.52547 3463 4.52495 3479 4.52444 3419 4.52393 3563 4.52341 3510 4.5229 3428 4.52239 3536 4.52188 3421 4.52136 3394 4.52085 3491 4.52034 3534 4.51982 3547 4.51931 3497 4.5188 3546 4.51828 3448 4.51777 3506 4.51726 3514 4.51675 3533 4.51623 3517 4.51572 3493 4.51521 3601 4.51469 3494 4.51418 3571 4.51367 3597 4.51315 3625 4.51264 3684 4.51213 3590 4.51162 3703 4.5111 3661 4.51059 3557 4.51008 3628 4.50956 3612 4.50905 3716 4.50854 3583 4.50803 3670 4.50751 3698 4.507 3557 4.50649 3681 4.50597 3698 4.50546 3677 4.50495 3668 4.50443 3688 4.50392 3716 4.50341 3718 4.50289 3659 4.50238 3674 4.50187 3653 4.50136 3710 4.50084 3594 4.50033 3702 4.49982 3589 4.4993 3570 4.49879 3651 4.49828 3661 4.49777 3689 4.49725 3779 4.49674 3604 4.49623 3700 4.49571 3697 4.4952 3698 4.49469 3686 4.49417 3685 4.49366 3693 4.49315 3686 4.49264 3684 4.49212 3746 4.49161 3669 4.4911 3688 4.49058 3748 4.49007 3718 4.48956 3724 4.48904 3756 4.48853 3797 4.48802 3863 4.48751 3847 4.48699 3762 4.48648 3687 4.48597 3799 4.48545 3769 4.48494 3731 4.48443 3794 4.48391 3779 4.4834 3766 4.48289 3764 4.48238 3781 4.48186 3949 4.48135 3831 4.48084 3904 4.48032 3857 4.47981 3943 4.4793 3828 4.47878 3806 4.47827 3835 4.47776 3951 4.47725 4043 4.47673 3905 4.47622 3864 4.47571 4010 4.47519 4086 4.47468 4025 4.47417 3971 4.47365 4012 4.47314 4104 4.47263 4081 4.47212 4024 4.4716 3985 4.47109 4011 4.47058 3985 4.47006 3884 4.46955 4030 4.46904 3944 4.46852 3965 4.46801 3944 4.4675 3902 4.46699 3957 4.46647 4050 4.46596 3973 4.46545 3961 4.46493 3924 4.46442 3956 4.46391 3949 4.46339 3968 4.46288 3982 4.46237 3976 4.46186 4052 4.46134 4035 4.46083 3964 4.46032 4011 4.4598 4010 4.45929 4069 4.45878 4052 4.45826 4021 4.45775 4087 4.45724 3998 4.45673 3896 4.45621 3993 4.4557 4042 4.45519 4159 4.45467 3967 4.45416 4093 4.45365 4124 4.45313 4060 4.45262 4089 4.45211 4127 4.4516 4088 4.45108 4069 4.45057 4146 4.45006 4190 4.44954 4201 4.44903 4167 4.44852 4199 4.448 4304 4.44749 4236 4.44698 4169 4.44647 4283 4.44595 4285 4.44544 4208 4.44493 4253 4.44441 4285 4.4439 4246 4.44339 4196 4.44287 4164 4.44236 4263 4.44185 4280 4.44134 4441 4.44082 4358 4.44031 4316 4.4398 4426 4.43928 4427 4.43877 4428 4.43826 4506 4.43775 4537 4.43723 4405 4.43672 4400 4.43621 4437 4.43569 4428 4.43518 4532 4.43467 4549 4.43415 4334 4.43364 4438 4.43313 4469 4.43262 4390 4.4321 4402 4.43159 4313 4.43108 4427 4.43056 4429 4.43005 4391 4.42954 4385 4.42902 4380 4.42851 4458 4.428 4455 4.42748 4408 4.42697 4486 4.42646 4455 4.42595 4403 4.42543 4408 4.42492 4459 4.42441 4495 4.42389 4488 4.42338 4439 4.42287 4429 4.42236 4507 4.42184 4507 4.42133 4466 4.42082 4479 4.4203 4554 4.41979 4571 4.41928 4523 4.41876 4480 4.41825 4566 4.41774 4624 4.41723 4586 4.41671 4585 4.4162 4601 4.41569 4551 4.41652 4568 4.41746 4535 4.41841 4583 4.41936 4590 4.4203 4653 4.42125 4690 4.4222 4644 4.42315 4651 4.42409 4789 4.42504 4777 4.42599 4716 4.42694 4701 4.42788 4795 4.42883 4880 4.42978 4802 4.43073 4719 4.43167 4891 4.43262 4862 4.43357 4869 4.43451 4879 4.43546 4810 4.43641 4933 4.43736 4861 4.4383 4780 4.43925 4868 4.4402 4924 4.44115 4928 4.44209 4911 4.44304 4942 4.44399 4866 4.44494 4820 4.44588 4765 4.44683 4773 4.44778 4751 4.44873 4819 4.44967 4651 4.45062 4741 4.45157 4748 4.45251 4824 4.45346 5064 4.45441 5120 4.45536 5277 4.4563 5372 4.45725 5342 4.4582 5547 4.45915 5752 4.46009 5669 4.46104 5696 4.46199 5562 4.46294 5217 4.46388 4879 4.46483 4683 4.46578 4608 4.46672 4605 4.46767 4365 4.46862 4136 4.46957 4058 4.47051 3706 4.47146 3271 4.47241 2953 4.47336 2721 4.4743 2573 4.47525 2491 4.4762 2402 4.47715 2439 4.47809 3127 4.47904 6427 4.47999 14945 4.48094 23205 4.48188 22864 4.48283 14406 4.48378 7388 4.48472 3783 4.48567 2320 4.48662 2025 4.48757 1924 4.48851 1945 4.48946 1977 4.49041 2017 4.49136 1925 4.4923 1920 4.49325 1935 4.4942 1945 4.49515 2046 4.49609 1956 4.49704 1982 4.49799 1908 4.49893 1977 4.49988 1907 4.50083 1995 4.50178 1979 4.50272 1881 4.50367 1969 4.50462 1953 4.50557 1980 4.50651 2000 4.50746 1961 4.50841 2002 4.50936 2113 4.5103 2029 4.51125 2003 4.5122 2052 4.51314 2008 4.51409 2029 4.51504 2035 4.51599 2099 4.51693 2029 4.51788 2014 4.51883 2031 4.51978 1963 4.52072 1993 4.52167 2074 4.52262 2015 4.52357 2091 4.52451 2094 4.52546 2095 4.52641 2126 4.52736 2138 4.5283 2097 4.52925 2056 4.5302 1990 4.53114 2135 4.53209 2005 4.53304 2075 4.53399 2228 4.53493 2069 4.53588 2130 4.53683 2307 4.53778 2354 4.53872 2281 4.53967 2317 4.54062 2325 4.54157 2224 4.54251 2205 4.54346 2112 4.54441 2106 4.54535 2027 4.5463 2052 4.54725 2033 4.5482 2038 4.54914 2012 4.55009 2012 4.55104 2054 4.55199 2047 4.55293 2078 4.55388 2038 4.55483 2000 4.55578 2039 4.55764 2078 4.5599 2078 4.56217 2079 4.56443 2091 4.56669 2074 4.56896 2022 4.57122 2075 4.57349 2006 4.57575 2034 4.57801 2055 4.58028 2102 4.58254 2138 4.58481 2084 4.58707 2179 4.58933 2126 4.5916 2117 4.59386 2078 4.59613 2155 4.59839 2135 4.60065 2103 4.60292 2186 4.60518 2169 4.60745 2065 4.60971 2103 4.61197 2192 4.61424 2119 4.6165 2177 4.61877 2148 4.62103 2180 4.62329 2100 4.62556 2147 4.62782 2218 4.63009 2169 4.63235 2212 4.63461 2227 4.63688 2109 4.63914 2136 4.64141 2167 4.64367 2184 4.64593 2249 4.6482 2107 4.65046 2185 4.65273 2291 4.65499 2264 4.65725 2191 4.65952 2245 4.66178 2278 4.66405 2282 4.66631 2250 4.66857 2257 4.67084 2402 4.6731 2444 4.67537 2399 4.67763 2427 4.67989 2297 4.68216 2272 4.68442 2312 4.68669 2294 4.68895 2409 4.69121 2304 4.69348 2168 4.69574 2266 4.69801 2285 4.70027 2197 4.70253 2314 4.7048 2317 4.70706 2228 4.70933 2328 4.71159 2349 4.71385 2583 4.71612 2862 4.71838 3222 4.72065 3269 4.72291 3077 4.72517 2700 4.72744 2274 4.7297 2214 4.73197 2031 4.73423 2082 4.73649 1986 4.73876 2012 4.74102 1988 4.74329 2024 4.74555 2167 4.74781 2286 4.75008 2798 4.75234 3412 4.75461 3968 4.75687 3735 4.75913 3040 4.7614 2391 4.76366 2073 4.76593 1967 4.76819 1843 4.77045 1793 4.77272 1734 4.77498 1770 4.77725 1782 4.77951 1782 4.78177 1802 4.78404 1666 4.7863 1773 4.78857 1675 4.79083 1824 4.79309 1731 4.79536 1817 4.79762 1786 4.79989 1747 4.80215 1755 4.80441 1722 4.80668 1800 4.80894 1742 4.81121 1765 4.81347 1703 4.81573 1742 4.818 1755 4.82026 1738 4.82253 1748 4.82479 1766 4.82705 1747 4.82932 1713 4.83158 1818 4.83385 1797 4.83611 1790 4.83837 1786 4.84064 1791 4.8429 1798 4.84517 1789 4.84743 1835 4.84969 1754 4.85196 1706 4.85422 1801 4.85648 1878 4.85875 1792 4.86101 1806 4.86328 1883 4.86554 1850 4.86781 1872 4.87007 1828 4.87233 1897 4.8746 1874 4.87686 1826 4.87913 1889 4.88139 1870 4.88365 1845 4.88592 1860 4.88818 1845 4.89044 1882 4.89271 1847 4.89497 1858 4.89724 1864 4.8995 1830 4.90176 1938 4.90403 1873 4.90629 1832 4.90856 1826 4.91082 1953 4.91308 1924 4.91535 1928 4.91761 1835 4.91988 1876 4.92214 1888 4.9244 1953 4.92667 2006 4.92893 2003 4.9312 2034 4.93346 2186 4.93572 2334 4.93799 2356 4.94025 2341 4.94252 2119 4.94478 1946 4.94704 1919 4.94931 1879 4.95157 1867 4.95384 1904 4.9561 1898 4.95836 1956 4.96063 1929 4.96289 1912 4.96516 1861 4.96742 1931 4.96968 1893 4.97195 1858 4.97421 1874 4.97648 2004 4.97874 1889 4.981 1927 4.98327 1945 4.98553 1957 4.9878 1917 4.99006 1952 4.99232 1923 4.99459 1998 4.99685 1959 4.99912 2004 5.00138 2023 5.00364 1987 5.00591 1985 5.00817 1999 5.01044 2063 5.01342 2043 5.01665 2006 5.01988 2070 5.02311 2009 5.02633 2079 5.02956 2033 5.03279 2040 5.03601 2053 5.03924 2053 5.04247 1996 5.0457 2010 5.04892 2054 5.05215 2001 5.05538 2039 5.05861 2113 5.06183 2080 5.06506 2124 5.06829 2100 5.07152 2094 5.07474 2147 5.07797 2158 5.0812 2230 5.08442 2139 5.08765 2151 5.09088 2189 5.09411 2284 5.09733 2196 5.10056 2266 5.10379 2272 5.10702 2292 5.11024 2279 5.11347 2273 5.1167 2182 5.11993 2059 5.12315 1991 5.12638 2018 5.12961 2014 5.13283 1842 5.13606 1938 5.13929 2103 5.14252 2632 5.14574 3783 5.14897 4606 5.1522 4725 5.15543 5238 5.15865 4911 5.16188 3258 5.16511 1853 5.16834 1496 5.17156 1545 5.17479 1452 5.17802 1479 5.18124 1569 5.18447 1576 5.1877 1532 5.19093 1508 5.19415 1524 5.19738 1466 5.20061 1457 5.20384 1434 5.20706 1463 5.21029 1525 5.21352 1518 5.21675 1490 5.21997 1419 5.2232 1489 5.22643 1479 5.22965 1487 5.23288 1542 5.23611 1518 5.23934 1506 5.24256 1521 5.24579 1575 5.24902 1574 5.25225 1651 5.25547 1720 5.2587 1673 5.26193 1699 5.26516 1656 5.26838 1706 5.27161 1649 5.27484 1621 5.27806 1568 5.28129 1531 5.28452 1433 5.28775 1437 5.29097 1350 5.2942 1245 5.29743 1228 5.30066 1135 5.30388 1143 5.30711 1151 5.31034 1213 5.31381 1240 5.31803 1534 5.32226 2206 5.32648 3379 5.33071 4727 5.33493 5137 5.33916 3777 5.34338 2370 5.34761 1611 5.35183 1246 5.35606 1159 5.36028 1206 5.36451 1132 5.36873 1106 5.37296 1052 5.37718 1115 5.38141 1089 5.38564 1051 5.38986 1110 5.39409 1110 5.39831 1072 5.40254 1058 5.40676 1046 5.41099 1017 5.41521 998 5.41944 1027 5.42366 1001 5.42789 1014 5.43211 1083 5.43634 1031 5.44056 1060 5.44479 1187 5.44902 1154 5.45324 1162 5.45747 1229 5.46169 1214 5.46592 1175 5.47014 1154 5.47437 1155 5.47859 1165 5.48282 1166 5.48704 1117 5.49127 1057 5.49549 988 5.49972 935 5.50394 799 5.50817 754 5.5124 687 5.51662 608 5.52085 593 5.52507 593 5.5293 584 5.53352 748 5.53775 1263 5.54197 2711 5.5462 4934 5.55042 5391 5.55465 3375 5.55887 1304 5.5631 621 5.56732 524 5.57155 529 5.57578 571 5.58 544 5.58423 523 5.58845 522 5.59268 525 5.5969 541 5.60113 521 5.60535 560 5.60958 590 5.6138 556 5.61803 564 5.62225 564 5.62648 526 5.6307 562 5.63493 556 5.63916 563 5.64338 638 5.64761 613 5.65183 573 5.65606 593 5.66028 548 5.66451 607 5.66873 674 5.67296 663 5.67718 666 5.68141 639 5.68563 631 5.68986 685 5.69408 705 5.69831 695 5.70254 604 5.70676 598 5.71099 582 5.71521 558 5.71944 602 5.72366 691 5.72789 641 5.73211 619 5.73634 613 5.74056 527 5.74479 551 5.74901 579 5.75324 513 5.75746 543 5.76169 541 5.76591 571 5.77014 551 5.77437 578 5.77859 540 5.78282 527 5.78704 520 5.79127 512 5.79549 510 5.79972 466 5.80394 477 5.80817 464 5.81239 489 5.81662 582 5.82084 593 5.82507 746 5.8293 887 5.83352 933 5.83775 846 5.84197 589 5.8462 464 5.85042 422 5.85465 413 5.85887 457 5.8631 518 5.86732 742 5.87155 969 5.87577 1161 5.87603 1197 5.87603 1009 5.87603 708 5.87603 440 5.87603 341 5.87603 225 5.87603 148 5.87603 126 5.87603 132 5.87603 184 5.87603 244 5.87603 309 5.87603 282 5.87603 304 5.87603 309 5.87603 324 5.87603 393 5.87603 470 5.87603 409 5.87603 378 5.87603 263 5.87603 170 5.87603 115 5.87603 55 5.87603 25 5.87603 6 5.87603 8 5.87603 6 5.87603 O 1s/2 nb_sba10.vms 2015 12 10 7 20 12 0 13 Casa Info Follows 1 Calib M = 281.718 A = 284.6 BE ADD 0 1 CASA region (*O 1s*) (*Shirley*) 943.808 963.808 0.78 2 0 0 299 542 275 9.3 (*O 1s*) 15.9994 0 2 CASA comp (*O 1s*) (*GL(30)*) Area 53167.692 0.001 10000000 -1 1 MFWHM 2.0463443 0.42 10.5 -1 1 Position 954.05538 943.808 963.808 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) CASA comp (*O 1s*) (*GL(30)*) Area 6286.9272 0.001 10000000 -1 1 MFWHM 1.4916421 0.42 10.5 -1 1 Position 956.36281 943.808 963.808 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) nb_sba10.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 666 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 332 Charge Neutraliser :On Acquired On :15/12/10 07:20:12 XPS 71 5 0 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 O 1s -1 Kinetic Energy eV 946.69 0.1 2 Intensity d Transmission d pulse counting 0.3315 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 4767 87285 1.31473 1.31659 8404 1.31659 8202 1.31658 8132 1.31657 7955 1.31656 7834 1.31655 7866 1.31654 7738 1.31653 7402 1.31652 7509 1.31651 7377 1.3165 7228 1.3165 7240 1.31649 7037 1.31648 6936 1.31647 6833 1.31646 6986 1.31645 6743 1.31644 6766 1.31643 6697 1.31642 6653 1.31641 6600 1.3164 6586 1.31639 6488 1.31638 6480 1.31637 6584 1.31637 6496 1.31636 6477 1.31635 6487 1.31634 6380 1.31633 6435 1.31632 6311 1.31631 6321 1.3163 6317 1.31629 6372 1.31628 6408 1.31627 6307 1.31626 6359 1.31625 6124 1.31624 6148 1.31623 6201 1.31623 6207 1.31622 6232 1.31621 6112 1.3162 6156 1.31619 6085 1.31618 6047 1.31617 6135 1.31616 6006 1.31615 6008 1.31614 5952 1.31613 5925 1.31612 6062 1.31611 5870 1.3161 6043 1.3161 5920 1.31609 5752 1.31608 5812 1.31607 5896 1.31606 5970 1.31605 5862 1.31604 5845 1.31603 5950 1.31602 5883 1.31601 6003 1.316 6197 1.31599 6155 1.31598 6366 1.31597 6498 1.31597 6664 1.31596 6529 1.31595 6892 1.31594 7112 1.31593 7315 1.31592 7807 1.31591 8418 1.3159 8903 1.31589 9491 1.31588 10219 1.31587 10856 1.31586 11949 1.31585 12927 1.31584 14492 1.31584 15736 1.31583 17532 1.31582 19456 1.31581 21584 1.3158 24141 1.31579 26598 1.31578 29767 1.31577 33401 1.31576 37113 1.31575 41105 1.31574 45693 1.31573 50338 1.31572 55383 1.31571 60763 1.3157 65868 1.3157 71124 1.31569 75210 1.31568 79507 1.31567 83360 1.31566 85590 1.31565 86871 1.31564 87285 1.31563 86227 1.31562 83367 1.31561 80374 1.3156 76178 1.31559 71421 1.31558 65852 1.31557 60607 1.31557 54293 1.31556 49277 1.31555 44525 1.31554 40630 1.31553 36403 1.31552 33740 1.31551 31172 1.3155 29202 1.31549 27807 1.31548 26370 1.31547 25417 1.31546 24377 1.31545 23589 1.31544 22600 1.31544 21582 1.31543 20715 1.31542 19647 1.31541 18304 1.3154 16947 1.31539 15693 1.31538 14308 1.31537 13079 1.31536 11821 1.31535 10757 1.31534 9663 1.31533 8978 1.31532 8019 1.31531 7430 1.31531 7148 1.3153 6554 1.31529 6357 1.31528 5929 1.31527 5724 1.31526 5686 1.31525 5564 1.31524 5303 1.31523 5221 1.31522 5266 1.31521 5261 1.3152 5164 1.31519 5125 1.31518 5076 1.31517 5001 1.31517 5075 1.31516 4953 1.31515 5010 1.31514 5114 1.31513 4911 1.31512 4859 1.31511 4881 1.3151 4899 1.31509 4972 1.31508 5100 1.31507 4875 1.31506 4867 1.31505 4824 1.31504 4863 1.31504 4876 1.31503 4923 1.31502 4915 1.31501 4886 1.315 4951 1.31499 4854 1.31498 4968 1.31497 4950 1.31496 4904 1.31495 4851 1.31494 4879 1.31493 4870 1.31492 4918 1.31491 4927 1.31491 4856 1.3149 4829 1.31489 4861 1.31488 4877 1.31487 4859 1.31486 4767 1.31485 4835 1.31484 4816 1.31483 4863 1.31482 4908 1.31481 4927 1.3148 4812 1.31479 4965 1.31478 5012 1.31478 4826 1.31477 4892 1.31476 4802 1.31475 4796 1.31474 4888 1.31473 C 1s/3 nb_sba10.vms 2015 12 10 7 20 12 0 13 Casa Info Follows 1 Calib M = 281.718 A = 284.6 BE ADD 0 1 CASA region (*C 1s*) (*Shirley*) 1183.808 1213.808 0.278 2 0 0 299 542 275 9.3 (*C 1s*) 12.011 0 2 CASA comp (*C 1s*) (*GL(30)*) Area 729.05192 0.001 10000000 -1 1 MFWHM 1.7862627 0.44 11 -1 1 Position 1202.1084 1183.808 1213.808 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) CASA comp (*C 1s*) (*GL(30)*) Area 688.6347 0.001 10000000 -1 1 MFWHM 4.0100004 0.57453967 14.363492 -1 1 Position 1200.1536 1183.808 1213.808 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) nb_sba10.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 782 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 260 Charge Neutraliser :On Acquired On :15/12/10 07:20:12 XPS 71 5 0 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 C 1s -1 Kinetic Energy eV 1186.69 0.1 2 Intensity d Transmission d pulse counting 0.2597 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 602 3095 4489 1.23374 1.24606 3281 1.24606 3229 1.24602 3332 1.24598 3214 1.24594 3338 1.2459 3272 1.24586 3244 1.24581 3208 1.24577 3299 1.24573 3268 1.24569 3237 1.24565 3297 1.24561 3243 1.24557 3322 1.24553 3314 1.24549 3296 1.24544 3198 1.2454 3364 1.24536 3219 1.24532 3284 1.24528 3305 1.24524 3128 1.2452 3319 1.24516 3250 1.24512 3269 1.24507 3270 1.24503 3351 1.24499 3249 1.24495 3286 1.24491 3375 1.24487 3243 1.24483 3107 1.24479 3236 1.24475 3245 1.24471 3177 1.24466 3328 1.24462 3139 1.24458 3168 1.24454 3309 1.2445 3190 1.24446 3290 1.24442 3101 1.24438 3373 1.24434 3246 1.24429 3253 1.24425 3235 1.24421 3312 1.24417 3333 1.24413 3179 1.24409 3335 1.24405 3259 1.24401 3251 1.24397 3302 1.24392 3264 1.24388 3186 1.24384 3173 1.2438 3277 1.24376 3318 1.24372 3136 1.24368 3216 1.24364 3243 1.2436 3312 1.24355 3136 1.24351 3352 1.24347 3177 1.24343 3196 1.24339 3147 1.24335 3186 1.24331 3294 1.24327 3244 1.24323 3272 1.24319 3275 1.24314 3237 1.2431 3270 1.24306 3303 1.24302 3297 1.24298 3286 1.24294 3228 1.2429 3266 1.24286 3363 1.24282 3194 1.24277 3294 1.24273 3281 1.24269 3255 1.24265 3259 1.24261 3278 1.24257 3148 1.24253 3230 1.24249 3314 1.24245 3287 1.2424 3289 1.24236 3147 1.24232 3307 1.24228 3229 1.24224 3265 1.2422 3314 1.24216 3149 1.24212 3208 1.24208 3267 1.24203 3203 1.24199 3199 1.24195 3300 1.24191 3161 1.24187 3216 1.24183 3275 1.24179 3222 1.24175 3248 1.24171 3249 1.24167 3269 1.24162 3250 1.24158 3294 1.24154 3273 1.2415 3277 1.24146 3288 1.24142 3334 1.24138 3364 1.24134 3245 1.2413 3228 1.24125 3270 1.24121 3234 1.24117 3249 1.24113 3263 1.24109 3155 1.24105 3450 1.24101 3339 1.24097 3287 1.24093 3375 1.24088 3464 1.24084 3440 1.2408 3501 1.24076 3287 1.24072 3324 1.24068 3355 1.24064 3353 1.2406 3416 1.24056 3447 1.24051 3411 1.24047 3435 1.24043 3436 1.24039 3458 1.24035 3430 1.24031 3432 1.24027 3413 1.24023 3524 1.24019 3480 1.24015 3575 1.2401 3470 1.24006 3516 1.24002 3392 1.23998 3567 1.23994 3447 1.2399 3511 1.23986 3525 1.23982 3463 1.23978 3610 1.23973 3713 1.23969 3684 1.23965 3603 1.23961 3651 1.23957 3667 1.23953 3657 1.23949 3679 1.23945 3723 1.23941 3711 1.23936 3805 1.23932 3691 1.23928 3809 1.23924 3793 1.2392 3685 1.23916 3955 1.23912 3875 1.23908 3944 1.23904 4083 1.23899 3996 1.23895 4124 1.23891 4226 1.23887 4188 1.23883 4215 1.23879 4195 1.23875 4244 1.23871 4269 1.23867 4336 1.23863 4465 1.23858 4388 1.23854 4489 1.2385 4349 1.23846 4430 1.23842 4250 1.23838 4245 1.23834 4032 1.2383 3972 1.23826 3861 1.23821 3778 1.23817 3777 1.23813 3643 1.23809 3532 1.23805 3503 1.23801 3514 1.23797 3354 1.23793 3322 1.23789 3309 1.23784 3210 1.2378 3257 1.23776 3277 1.23772 3202 1.23768 3262 1.23764 3124 1.2376 3261 1.23756 3270 1.23752 3203 1.23747 3233 1.23743 3215 1.23739 3207 1.23735 3181 1.23731 3160 1.23727 3245 1.23723 3325 1.23719 3163 1.23715 3336 1.23711 3170 1.23706 3176 1.23702 3214 1.23698 3159 1.23694 3254 1.2369 3211 1.23686 3244 1.23682 3184 1.23678 3304 1.23674 3288 1.23669 3299 1.23665 3234 1.23661 3248 1.23657 3173 1.23653 3352 1.23649 3266 1.23645 3095 1.23641 3191 1.23637 3216 1.23632 3299 1.23628 3146 1.23624 3287 1.2362 3176 1.23616 3175 1.23612 3352 1.23608 3201 1.23604 3131 1.236 3272 1.23595 3288 1.23591 3277 1.23587 3209 1.23583 3119 1.23579 3163 1.23575 3265 1.23571 3296 1.23567 3272 1.23563 3237 1.23559 3253 1.23554 3171 1.2355 3186 1.23546 3189 1.23542 3179 1.23538 3300 1.23534 3153 1.2353 3229 1.23526 3208 1.23522 3244 1.23517 3361 1.23513 3176 1.23509 3277 1.23505 3282 1.23501 3253 1.23497 3286 1.23493 3129 1.23489 3151 1.23485 3193 1.2348 3280 1.23476 3194 1.23472 3169 1.23468 3299 1.23464 3313 1.2346 3270 1.23456 3230 1.23452 3168 1.23448 3194 1.23443 3170 1.23439 3189 1.23435 3179 1.23431 3256 1.23427 3297 1.23423 3243 1.23419 3339 1.23415 3142 1.23411 3240 1.23407 3222 1.23402 3308 1.23398 3145 1.23394 3252 1.2339 3140 1.23386 3208 1.23382 3139 1.23378 3201 1.23374 Nb 3d/4 nb_sba10.vms 2015 12 10 7 20 12 0 13 Casa Info Follows 1 Calib M = 281.718 A = 284.6 BE ADD 0 1 CASA region (*Nb 3d*) (*Shirley*) 1271.808 1283.0231 2.921 2 0 0 299 542 275 9.3 (*Nb 3d*) 92.9064 0 2 CASA comp (*Nb 3d*) (*GL(30)*) Area 6115.5611 0.001 10000000 -1 1 MFWHM 1.5376488 0.36 9 -1 1 Position 1279.3601 1271.808 1288.808 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) CASA comp (*Nb 3d*) (*GL(30)*) Area 5357.7546 0.001 10000000 -1 1 MFWHM 2.0242114 0.36 9 -1 1 Position 1276.6809 1271.808 1288.808 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) nb_sba10.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 2350 Sweeps: 30 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 458 Charge Neutraliser :On Acquired On :15/12/10 07:20:12 XPS 71 5 0 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Nb 3d -1 Kinetic Energy eV 1274.69 0.1 2 Intensity d Transmission d pulse counting 0.458 30 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 342 12388 64380 1.20664 1.21249 16703 1.21249 16822 1.21245 16742 1.21242 16566 1.21239 16579 1.21235 16524 1.21232 16694 1.21228 16608 1.21225 16649 1.21221 16690 1.21218 16671 1.21214 16637 1.21211 16722 1.21208 16638 1.21204 16719 1.21201 16763 1.21197 16754 1.21194 16827 1.2119 17091 1.21187 17295 1.21183 17655 1.2118 17633 1.21177 17625 1.21173 18131 1.2117 18516 1.21166 18787 1.21163 19478 1.21159 19657 1.21156 20287 1.21152 21166 1.21149 21539 1.21146 22593 1.21142 23416 1.21139 24350 1.21135 25546 1.21132 26396 1.21128 27672 1.21125 29444 1.21121 31449 1.21118 32829 1.21115 34980 1.21111 37041 1.21108 39315 1.21104 41748 1.21101 44077 1.21097 46128 1.21094 48083 1.2109 49987 1.21087 50464 1.21084 50540 1.2108 50606 1.21077 49190 1.21073 47463 1.2107 45296 1.21066 42807 1.21063 40583 1.21059 38185 1.21056 35695 1.21053 34333 1.21049 33119 1.21046 32679 1.21042 32089 1.21039 32259 1.21035 33338 1.21032 34468 1.21029 36565 1.21025 38679 1.21022 41496 1.21018 44572 1.21015 47250 1.21011 51129 1.21008 54504 1.21004 57627 1.21001 60161 1.20998 62686 1.20994 64380 1.20991 63760 1.20987 63738 1.20984 60821 1.2098 57746 1.20977 53642 1.20973 49051 1.2097 44287 1.20967 39546 1.20963 34562 1.2096 30322 1.20956 26562 1.20953 23269 1.20949 20459 1.20946 18509 1.20942 16956 1.20939 15726 1.20936 14874 1.20932 14248 1.20929 13984 1.20925 13436 1.20922 13205 1.20918 13032 1.20915 13003 1.20911 13037 1.20908 12781 1.20905 12796 1.20901 12577 1.20898 12651 1.20894 12649 1.20891 12686 1.20887 12543 1.20884 12612 1.2088 12604 1.20877 12720 1.20874 12658 1.2087 12673 1.20867 12624 1.20863 12656 1.2086 12388 1.20856 12588 1.20853 12588 1.20849 12594 1.20846 12762 1.20843 12470 1.20839 12804 1.20836 12727 1.20832 12778 1.20829 12733 1.20825 12642 1.20822 12714 1.20819 12491 1.20815 12751 1.20812 12722 1.20808 12639 1.20805 12787 1.20801 12614 1.20798 12525 1.20794 12670 1.20791 12610 1.20788 12662 1.20784 12789 1.20781 12792 1.20777 12903 1.20774 12619 1.2077 12968 1.20767 12673 1.20763 12778 1.2076 12825 1.20757 12752 1.20753 12852 1.2075 12874 1.20746 12980 1.20743 12798 1.20739 12890 1.20736 12900 1.20732 12880 1.20729 12877 1.20726 13022 1.20722 12842 1.20719 12912 1.20715 12986 1.20712 13163 1.20708 13025 1.20705 12979 1.20701 12941 1.20698 13124 1.20695 12995 1.20691 13143 1.20688 12819 1.20684 13125 1.20681 13193 1.20677 12983 1.20674 13133 1.2067 12950 1.20667 13041 1.20664 Si 2p/5 nb_sba10.vms 2015 12 10 7 20 12 0 13 Casa Info Follows 1 Calib M = 281.718 A = 284.6 BE ADD 0 1 CASA region (*Si 2p*) (*Shirley*) 1373.808 1393.808 0.328 2 0 0 299 542 275 9.3 (*Si 2p*) 28.0858 0 2 CASA comp (*Si 2p*) (*GL(30)*) Area 7381.5654 0.001 10000000 -1 1 MFWHM 1.7028719 0.4 10 -1 1 Position 1383.4588 1373.808 1393.808 -1 1 RSF 0.328 MASS 28.0858 INDEX -1 (*Si 2p*) CONST (**) CASA comp (*Si 2p*) (*GL(30)*) Area 1527.1383 0.001 10000000 -1 1 MFWHM 1.9947501 0.38446329 9.6115822 -1 1 Position 1382.291 1373.808 1393.808 -1 1 RSF 0.328 MASS 28.0858 INDEX -1 (*Si 2p*) CONST (**) nb_sba10.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 799 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 397 Charge Neutraliser :On Acquired On :15/12/10 07:20:12 XPS 71 5 0 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Si 2p -1 Kinetic Energy eV 1376.69 0.1 2 Intensity d Transmission d pulse counting 0.3974 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 1168 18389 1.19156 1.19218 1681 1.19218 1687 1.19218 1655 1.19217 1712 1.19217 1601 1.19217 1579 1.19216 1613 1.19216 1589 1.19216 1555 1.19215 1570 1.19215 1491 1.19215 1541 1.19214 1549 1.19214 1462 1.19214 1523 1.19213 1473 1.19213 1383 1.19213 1510 1.19213 1443 1.19212 1436 1.19212 1416 1.19212 1436 1.19211 1399 1.19211 1456 1.19211 1398 1.1921 1379 1.1921 1489 1.1921 1417 1.19209 1370 1.19209 1341 1.19209 1384 1.19209 1333 1.19208 1325 1.19208 1325 1.19208 1369 1.19207 1348 1.19207 1360 1.19207 1397 1.19206 1353 1.19206 1363 1.19206 1346 1.19205 1283 1.19205 1273 1.19205 1364 1.19205 1274 1.19204 1290 1.19204 1313 1.19204 1324 1.19203 1336 1.19203 1299 1.19203 1315 1.19202 1356 1.19202 1320 1.19202 1302 1.19201 1305 1.19201 1415 1.19201 1319 1.19201 1403 1.192 1508 1.192 1477 1.192 1515 1.19199 1588 1.19199 1573 1.19199 1758 1.19198 1718 1.19198 1790 1.19198 1957 1.19197 1997 1.19197 2135 1.19197 2296 1.19196 2419 1.19196 2656 1.19196 2827 1.19196 3000 1.19195 3271 1.19195 3444 1.19195 3784 1.19194 4103 1.19194 4527 1.19194 4864 1.19193 5318 1.19193 5878 1.19193 6632 1.19192 7230 1.19192 8245 1.19192 8944 1.19192 10206 1.19191 11082 1.19191 12186 1.19191 13227 1.1919 14364 1.1919 15639 1.1919 16524 1.19189 17324 1.19189 18038 1.19189 18055 1.19188 18389 1.19188 18100 1.19188 17813 1.19188 17000 1.19187 16135 1.19187 15051 1.19187 13614 1.19186 12340 1.19186 10726 1.19186 9563 1.19185 8137 1.19185 7022 1.19185 5936 1.19184 5147 1.19184 4277 1.19184 3634 1.19184 3174 1.19183 2747 1.19183 2340 1.19183 2100 1.19182 1853 1.19182 1706 1.19182 1644 1.19181 1540 1.19181 1461 1.19181 1351 1.1918 1337 1.1918 1333 1.1918 1297 1.1918 1380 1.19179 1263 1.19179 1266 1.19179 1278 1.19178 1243 1.19178 1193 1.19178 1264 1.19177 1204 1.19177 1219 1.19177 1263 1.19176 1268 1.19176 1271 1.19176 1195 1.19176 1245 1.19175 1395 1.19175 1256 1.19175 1218 1.19174 1224 1.19174 1175 1.19174 1222 1.19173 1312 1.19173 1255 1.19173 1172 1.19172 1250 1.19172 1224 1.19172 1263 1.19171 1269 1.19171 1203 1.19171 1312 1.19171 1265 1.1917 1207 1.1917 1283 1.1917 1181 1.19169 1225 1.19169 1197 1.19169 1176 1.19168 1189 1.19168 1214 1.19168 1209 1.19167 1232 1.19167 1277 1.19167 1176 1.19167 1328 1.19166 1209 1.19166 1205 1.19166 1263 1.19165 1234 1.19165 1267 1.19165 1194 1.19164 1168 1.19164 1262 1.19164 1197 1.19163 1176 1.19163 1233 1.19163 1226 1.19163 1224 1.19162 1348 1.19162 1267 1.19162 1218 1.19161 1243 1.19161 1209 1.19161 1280 1.1916 1244 1.1916 1187 1.1916 1285 1.19159 1199 1.19159 1207 1.19159 1200 1.19159 1294 1.19158 1245 1.19158 1222 1.19158 1279 1.19157 1207 1.19157 1201 1.19157 1289 1.19156 1248 1.19156 wide/1 nb_sba2.vms 2015 12 10 2 28 44 0 11 Casa Info Follows 2 Calib M = 281.1 A = 284.6 BE ADD Calib M = 284.648 A = 284.6 BE ADD 0 0 0 nb_sba2.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 160 Acqn. Time(s): 603 Sweeps: 5 Anode:Mono(Al (Mono))(156 W) Step(meV): 1000.0 Dwell Time(ms): 100 Charge Neutraliser :On Acquired On :15/12/10 02:28:44 XPS 46 7 1 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 160 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Wide None -1 Kinetic Energy eV 286.69 1 2 Intensity d Transmission d pulse counting 0.1 5 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 2412 2 17290 4.41569 8.42235 2104 8.42235 2104 8.38839 2074 8.35442 2078 8.32045 2102 8.28649 2112 8.25252 2030 8.21856 2043 8.18459 2047 8.15063 2088 8.11666 2110 8.0827 2085 8.04873 2109 8.01476 2060 7.9808 2125 7.94683 2119 7.91287 2099 7.8789 2106 7.84494 2090 7.81097 2020 7.77701 2124 7.74304 2112 7.70907 2130 7.67511 2162 7.64114 2113 7.60718 2170 7.57321 2213 7.53925 2172 7.50528 2153 7.47131 2181 7.43735 2124 7.40338 2206 7.36942 2153 7.33545 2160 7.30149 2129 7.26752 2130 7.23356 2155 7.19959 2147 7.16562 2067 7.13166 2155 7.09769 2172 7.06373 2172 7.02976 2096 7.00512 2187 6.99202 2186 6.97893 2224 6.96583 2189 6.95273 2163 6.93963 2213 6.92653 2235 6.91343 2150 6.90033 2220 6.88723 2274 6.87414 2254 6.86104 2179 6.84794 2251 6.83484 2181 6.82174 2251 6.80864 2213 6.79554 2152 6.78244 2255 6.76935 2244 6.75625 2241 6.74315 2273 6.73005 2239 6.71695 2290 6.70385 2256 6.69075 2224 6.67765 2249 6.66456 2325 6.65146 2331 6.63836 2348 6.62526 2349 6.61216 2290 6.59906 2344 6.58596 2271 6.57286 2335 6.55976 2319 6.54667 2321 6.53357 2313 6.52047 2297 6.50737 2357 6.49427 2365 6.48117 2377 6.46807 2366 6.45497 2408 6.44188 2300 6.42878 2444 6.41568 2314 6.40258 2370 6.38948 2407 6.37638 2415 6.36328 2344 6.35018 2395 6.33709 2417 6.32399 2426 6.31089 2454 6.29779 2363 6.28469 2420 6.27159 2418 6.25849 2459 6.24539 2431 6.2323 2421 6.2192 2399 6.2061 2439 6.193 2510 6.1799 2431 6.1668 2451 6.1537 2435 6.1406 2465 6.1275 2414 6.11441 2474 6.10131 2490 6.08821 2469 6.07511 2498 6.06201 2474 6.04891 2482 6.03581 2503 6.02271 2406 6.00962 2446 5.99652 2565 5.98342 2510 5.97032 2583 5.95722 2507 5.94412 2504 5.93102 2535 5.91792 2521 5.90483 2578 5.89173 2581 5.87863 2541 5.86553 2570 5.85243 2608 5.83933 2557 5.82623 2605 5.81313 2602 5.80004 2622 5.78694 2619 5.77384 2741 5.76074 2680 5.74764 2595 5.73454 2671 5.72144 2634 5.70834 2632 5.69524 2641 5.68215 2665 5.66905 2707 5.65595 2669 5.64285 2613 5.62975 2700 5.61665 2655 5.60355 2707 5.59045 2729 5.57736 2724 5.56426 2746 5.55116 2734 5.53806 2786 5.52496 2792 5.51186 2810 5.49876 2762 5.48566 2783 5.47257 2894 5.45947 2798 5.44637 2863 5.43327 2796 5.42017 2782 5.40707 2828 5.39397 2828 5.38087 2838 5.36778 2821 5.35468 2783 5.34158 2813 5.33457 2900 5.33071 2886 5.32684 2821 5.32297 2910 5.31911 2866 5.31524 3001 5.31137 2969 5.30751 2920 5.30364 3003 5.29978 3076 5.29591 2915 5.29204 3096 5.28818 3050 5.28431 2996 5.28044 3114 5.27658 3269 5.27271 3261 5.26885 3137 5.26498 3083 5.26111 3026 5.25725 2975 5.25338 3037 5.24951 3106 5.24565 3071 5.24178 3082 5.23792 3236 5.23405 3213 5.23018 3390 5.22632 3397 5.22245 3518 5.21858 3599 5.21472 3576 5.21085 3571 5.20699 3461 5.20312 3363 5.19925 3328 5.19539 3127 5.19152 3124 5.18765 3183 5.18379 3060 5.17992 2897 5.17606 2934 5.17219 2921 5.16832 3119 5.16446 3096 5.16059 2980 5.15672 3073 5.15286 3374 5.14899 3736 5.14513 3946 5.14126 4106 5.13739 4484 5.13353 4785 5.12966 4754 5.12579 4401 5.12193 3836 5.11806 3429 5.1142 3144 5.11033 2847 5.10646 2681 5.1026 2443 5.09873 2370 5.09486 2191 5.091 2077 5.08713 1929 5.08327 1849 5.0794 1780 5.07553 1735 5.07167 1648 5.0678 1695 5.06393 1703 5.06007 1723 5.0562 1767 5.05234 1699 5.04847 1720 5.0446 1729 5.04074 1707 5.03687 1724 5.033 1717 5.02914 1683 5.02527 1718 5.02141 1757 5.01754 1737 5.01367 1654 5.00981 1705 5.00594 1745 5.00207 1768 4.99821 1723 4.99434 1728 4.99048 1679 4.98661 1740 4.98274 1723 4.97888 1770 4.97501 1736 4.97114 1728 4.96728 1748 4.96341 1736 4.95955 1754 4.95568 1742 4.95181 1701 4.94795 1760 4.94408 1763 4.94021 1841 4.93635 1801 4.93248 1758 4.92862 1786 4.92475 1818 4.92088 1794 4.91702 1741 4.91315 1740 4.90928 1785 4.90542 1759 4.90155 1768 4.89769 1757 4.89382 1787 4.88995 1797 4.88609 1832 4.88222 1831 4.87835 1742 4.87449 1773 4.87062 1782 4.86676 1770 4.86289 1847 4.85902 1824 4.85516 1837 4.85129 1801 4.84742 1773 4.84356 1780 4.83969 1854 4.83582 1859 4.83196 1828 4.82809 1788 4.82423 1837 4.82036 1817 4.81649 1850 4.81263 1843 4.80876 1889 4.80489 1839 4.80103 1879 4.79716 1840 4.7933 1845 4.78943 1873 4.78556 1786 4.7817 1895 4.77783 1845 4.77396 1881 4.7701 1892 4.76623 1868 4.76237 1896 4.7585 1822 4.75463 1927 4.75077 1890 4.7469 1871 4.74303 1945 4.73917 1874 4.7353 1907 4.73144 1850 4.72757 1927 4.7237 1956 4.71984 1947 4.71597 1887 4.7121 1916 4.70824 1875 4.70437 1893 4.70051 1890 4.69664 1920 4.69277 1895 4.68891 1872 4.68504 1968 4.68117 1986 4.67731 1937 4.67344 2007 4.66958 1974 4.66571 1912 4.66184 1958 4.65798 2053 4.65411 2093 4.65024 2034 4.64638 1949 4.64251 1937 4.63865 1969 4.63478 1891 4.63091 1931 4.62705 1974 4.62318 1871 4.61931 1927 4.61545 1932 4.61158 1943 4.60772 1905 4.60385 1947 4.59998 1965 4.59612 1925 4.59225 1854 4.58838 1903 4.58452 2004 4.58065 1961 4.57679 1973 4.57292 1931 4.56905 1948 4.56519 1976 4.56132 1953 4.55745 1941 4.55359 1959 4.54972 1982 4.54586 2015 4.54199 1995 4.53812 2025 4.53426 2064 4.53039 2037 4.52906 1978 4.52854 2049 4.52803 2041 4.52752 2104 4.52701 2065 4.52649 2073 4.52598 2002 4.52547 2100 4.52495 2050 4.52444 2016 4.52393 2051 4.52341 2038 4.5229 2012 4.52239 2071 4.52188 2055 4.52136 2036 4.52085 2037 4.52034 2062 4.51982 2066 4.51931 2096 4.5188 1996 4.51828 2035 4.51777 1992 4.51726 2070 4.51675 2089 4.51623 2095 4.51572 2080 4.51521 1994 4.51469 2089 4.51418 2091 4.51367 2074 4.51315 2112 4.51264 2067 4.51213 2069 4.51162 2156 4.5111 2137 4.51059 2092 4.51008 2090 4.50956 2131 4.50905 2126 4.50854 2107 4.50803 2086 4.50751 2082 4.507 2130 4.50649 2121 4.50597 2153 4.50546 2148 4.50495 2117 4.50443 2147 4.50392 2175 4.50341 2132 4.50289 2152 4.50238 2177 4.50187 2255 4.50136 2194 4.50084 2195 4.50033 2138 4.49982 2158 4.4993 2195 4.49879 2137 4.49828 2228 4.49777 2112 4.49725 2127 4.49674 2150 4.49623 2211 4.49571 2193 4.4952 2214 4.49469 2143 4.49417 2134 4.49366 2250 4.49315 2248 4.49264 2252 4.49212 2258 4.49161 2187 4.4911 2250 4.49058 2189 4.49007 2263 4.48956 2205 4.48904 2240 4.48853 2164 4.48802 2285 4.48751 2242 4.48699 2226 4.48648 2211 4.48597 2269 4.48545 2256 4.48494 2169 4.48443 2303 4.48391 2250 4.4834 2259 4.48289 2308 4.48238 2314 4.48186 2307 4.48135 2246 4.48084 2242 4.48032 2296 4.47981 2259 4.4793 2280 4.47878 2303 4.47827 2266 4.47776 2272 4.47725 2387 4.47673 2357 4.47622 2300 4.47571 2339 4.47519 2314 4.47468 2314 4.47417 2394 4.47365 2344 4.47314 2332 4.47263 2387 4.47212 2299 4.4716 2306 4.47109 2352 4.47058 2302 4.47006 2412 4.46955 2405 4.46904 2349 4.46852 2415 4.46801 2397 4.4675 2387 4.46699 2303 4.46647 2299 4.46596 2363 4.46545 2294 4.46493 2346 4.46442 2325 4.46391 2385 4.46339 2350 4.46288 2347 4.46237 2348 4.46186 2297 4.46134 2341 4.46083 2390 4.46032 2397 4.4598 2443 4.45929 2400 4.45878 2405 4.45826 2404 4.45775 2337 4.45724 2369 4.45673 2345 4.45621 2432 4.4557 2449 4.45519 2483 4.45467 2422 4.45416 2410 4.45365 2415 4.45313 2417 4.45262 2419 4.45211 2450 4.4516 2464 4.45108 2388 4.45057 2368 4.45006 2517 4.44954 2473 4.44903 2509 4.44852 2488 4.448 2580 4.44749 2466 4.44698 2490 4.44647 2511 4.44595 2501 4.44544 2515 4.44493 2479 4.44441 2435 4.4439 2462 4.44339 2509 4.44287 2519 4.44236 2529 4.44185 2442 4.44134 2513 4.44082 2575 4.44031 2580 4.4398 2539 4.43928 2578 4.43877 2575 4.43826 2534 4.43775 2488 4.43723 2577 4.43672 2569 4.43621 2529 4.43569 2544 4.43518 2697 4.43467 2607 4.43415 2553 4.43364 2576 4.43313 2527 4.43262 2565 4.4321 2681 4.43159 2637 4.43108 2641 4.43056 2576 4.43005 2606 4.42954 2521 4.42902 2640 4.42851 2630 4.428 2729 4.42748 2617 4.42697 2582 4.42646 2580 4.42595 2637 4.42543 2648 4.42492 2624 4.42441 2570 4.42389 2642 4.42338 2735 4.42287 2708 4.42236 2640 4.42184 2673 4.42133 2703 4.42082 2635 4.4203 2620 4.41979 2657 4.41928 2648 4.41876 2671 4.41825 2618 4.41774 2719 4.41723 2633 4.41671 2718 4.4162 2642 4.41569 2631 4.41652 2731 4.41746 2706 4.41841 2629 4.41936 2698 4.4203 2762 4.42125 2753 4.4222 2771 4.42315 2720 4.42409 2747 4.42504 2745 4.42599 2763 4.42694 2851 4.42788 2710 4.42883 2862 4.42978 2764 4.43073 2898 4.43167 2949 4.43262 2796 4.43357 2827 4.43451 2812 4.43546 2742 4.43641 2847 4.43736 2883 4.4383 2867 4.43925 2893 4.4402 2833 4.44115 2784 4.44209 2856 4.44304 2817 4.44399 2817 4.44494 2822 4.44588 2783 4.44683 2773 4.44778 2657 4.44873 2670 4.44967 2647 4.45062 2605 4.45157 2676 4.45251 2885 4.45346 2932 4.45441 3120 4.45536 3097 4.4563 3263 4.45725 3240 4.4582 3315 4.45915 3388 4.46009 3434 4.46104 3461 4.46199 3217 4.46294 3162 4.46388 2769 4.46483 2582 4.46578 2499 4.46672 2433 4.46767 2364 4.46862 2209 4.46957 2155 4.47051 1842 4.47146 1532 4.47241 1247 4.47336 1075 4.4743 984 4.47525 911 4.4762 915 4.47715 906 4.47809 1246 4.47904 3331 4.47999 9995 4.48094 17290 4.48188 16423 4.48283 8488 4.48378 2903 4.48472 1262 4.48567 900 4.48662 824 4.48757 826 4.48851 827 4.48946 807 4.49041 850 4.49136 748 4.4923 832 4.49325 793 4.4942 785 4.49515 788 4.49609 814 4.49704 809 4.49799 768 4.49893 750 4.49988 807 4.50083 774 4.50178 794 4.50272 808 4.50367 770 4.50462 757 4.50557 773 4.50651 791 4.50746 795 4.50841 804 4.50936 784 4.5103 777 4.51125 794 4.5122 789 4.51314 807 4.51409 828 4.51504 851 4.51599 808 4.51693 775 4.51788 768 4.51883 786 4.51978 787 4.52072 798 4.52167 792 4.52262 825 4.52357 788 4.52451 818 4.52546 801 4.52641 808 4.52736 824 4.5283 791 4.52925 808 4.5302 789 4.53114 793 4.53209 765 4.53304 762 4.53399 746 4.53493 807 4.53588 859 4.53683 835 4.53778 784 4.53872 815 4.53967 779 4.54062 845 4.54157 843 4.54251 844 4.54346 767 4.54441 792 4.54535 855 4.5463 819 4.54725 797 4.5482 772 4.54914 769 4.55009 810 4.55104 808 4.55199 788 4.55293 771 4.55388 787 4.55483 796 4.55578 772 4.55764 832 4.5599 858 4.56217 797 4.56443 766 4.56669 789 4.56896 817 4.57122 787 4.57349 810 4.57575 801 4.57801 794 4.58028 786 4.58254 804 4.58481 821 4.58707 837 4.58933 827 4.5916 803 4.59386 774 4.59613 847 4.59839 793 4.60065 810 4.60292 815 4.60518 822 4.60745 846 4.60971 858 4.61197 861 4.61424 779 4.6165 815 4.61877 836 4.62103 810 4.62329 856 4.62556 827 4.62782 817 4.63009 867 4.63235 835 4.63461 831 4.63688 764 4.63914 774 4.64141 799 4.64367 794 4.64593 769 4.6482 841 4.65046 857 4.65273 838 4.65499 817 4.65725 837 4.65952 813 4.66178 867 4.66405 856 4.66631 846 4.66857 849 4.67084 848 4.6731 873 4.67537 848 4.67763 873 4.67989 833 4.68216 852 4.68442 841 4.68669 832 4.68895 861 4.69121 824 4.69348 860 4.69574 831 4.69801 831 4.70027 872 4.70253 887 4.7048 836 4.70706 811 4.70933 904 4.71159 848 4.71385 870 4.71612 925 4.71838 931 4.72065 899 4.72291 864 4.72517 890 4.72744 872 4.7297 835 4.73197 822 4.73423 767 4.73649 845 4.73876 796 4.74102 785 4.74329 825 4.74555 802 4.74781 848 4.75008 881 4.75234 971 4.75461 1046 4.75687 986 4.75913 916 4.7614 841 4.76366 835 4.76593 838 4.76819 799 4.77045 828 4.77272 830 4.77498 810 4.77725 822 4.77951 807 4.78177 800 4.78404 772 4.7863 758 4.78857 793 4.79083 806 4.79309 801 4.79536 761 4.79762 825 4.79989 827 4.80215 801 4.80441 791 4.80668 812 4.80894 766 4.81121 813 4.81347 812 4.81573 789 4.818 810 4.82026 804 4.82253 782 4.82479 795 4.82705 817 4.82932 775 4.83158 793 4.83385 816 4.83611 851 4.83837 809 4.84064 797 4.8429 806 4.84517 803 4.84743 822 4.84969 800 4.85196 823 4.85422 846 4.85648 772 4.85875 801 4.86101 813 4.86328 817 4.86554 821 4.86781 826 4.87007 763 4.87233 820 4.8746 757 4.87686 808 4.87913 833 4.88139 834 4.88365 821 4.88592 811 4.88818 814 4.89044 839 4.89271 854 4.89497 842 4.89724 841 4.8995 807 4.90176 807 4.90403 832 4.90629 842 4.90856 817 4.91082 847 4.91308 872 4.91535 795 4.91761 810 4.91988 792 4.92214 810 4.9244 830 4.92667 834 4.92893 876 4.9312 863 4.93346 866 4.93572 917 4.93799 978 4.94025 992 4.94252 884 4.94478 814 4.94704 838 4.94931 830 4.95157 810 4.95384 816 4.9561 797 4.95836 826 4.96063 809 4.96289 789 4.96516 817 4.96742 808 4.96968 785 4.97195 825 4.97421 812 4.97648 849 4.97874 788 4.981 811 4.98327 855 4.98553 837 4.9878 844 4.99006 813 4.99232 812 4.99459 811 4.99685 833 4.99912 811 5.00138 852 5.00364 865 5.00591 837 5.00817 823 5.01044 826 5.01342 835 5.01665 850 5.01988 832 5.02311 864 5.02633 841 5.02956 886 5.03279 888 5.03601 845 5.03924 926 5.04247 876 5.0457 878 5.04892 858 5.05215 845 5.05538 835 5.05861 850 5.06183 842 5.06506 813 5.06829 875 5.07152 876 5.07474 827 5.07797 952 5.0812 902 5.08442 875 5.08765 893 5.09088 864 5.09411 854 5.09733 915 5.10056 895 5.10379 863 5.10702 891 5.11024 892 5.11347 906 5.1167 887 5.11993 872 5.12315 892 5.12638 847 5.12961 898 5.13283 901 5.13606 899 5.13929 927 5.14252 970 5.14574 1080 5.14897 1134 5.1522 1199 5.15543 1259 5.15865 1074 5.16188 967 5.16511 918 5.16834 812 5.17156 839 5.17479 883 5.17802 881 5.18124 866 5.18447 894 5.1877 908 5.19093 911 5.19415 877 5.19738 901 5.20061 929 5.20384 927 5.20706 859 5.21029 851 5.21352 902 5.21675 842 5.21997 805 5.2232 874 5.22643 880 5.22965 856 5.23288 903 5.23611 925 5.23934 925 5.24256 961 5.24579 1004 5.24902 924 5.25225 958 5.25547 1005 5.2587 1048 5.26193 1016 5.26516 978 5.26838 950 5.27161 943 5.27484 887 5.27806 895 5.28129 862 5.28452 811 5.28775 773 5.29097 728 5.2942 685 5.29743 645 5.30066 613 5.30388 624 5.30711 651 5.31034 550 5.31381 662 5.31803 764 5.32226 1185 5.32648 2015 5.33071 3268 5.33493 3565 5.33916 2677 5.34338 1539 5.34761 967 5.35183 742 5.35606 639 5.36028 610 5.36451 624 5.36873 625 5.37296 587 5.37718 602 5.38141 613 5.38564 570 5.38986 555 5.39409 551 5.39831 549 5.40254 559 5.40676 558 5.41099 538 5.41521 539 5.41944 551 5.42366 515 5.42789 536 5.43211 550 5.43634 622 5.44056 581 5.44479 608 5.44902 650 5.45324 630 5.45747 656 5.46169 656 5.46592 645 5.47014 619 5.47437 605 5.47859 549 5.48282 520 5.48704 519 5.49127 466 5.49549 442 5.49972 388 5.50394 331 5.50817 275 5.5124 239 5.51662 207 5.52085 194 5.52507 191 5.5293 209 5.53352 218 5.53775 428 5.54197 1472 5.5462 3321 5.55042 3774 5.55465 2233 5.55887 778 5.5631 256 5.56732 221 5.57155 176 5.57578 182 5.58 204 5.58423 179 5.58845 183 5.59268 177 5.5969 209 5.60113 197 5.60535 193 5.60958 217 5.6138 194 5.61803 207 5.62225 194 5.62648 195 5.6307 192 5.63493 192 5.63916 205 5.64338 187 5.64761 198 5.65183 203 5.65606 201 5.66028 184 5.66451 197 5.66873 213 5.67296 243 5.67718 236 5.68141 219 5.68563 215 5.68986 224 5.69408 227 5.69831 225 5.70254 213 5.70676 190 5.71099 206 5.71521 193 5.71944 215 5.72366 215 5.72789 214 5.73211 182 5.73634 193 5.74056 217 5.74479 232 5.74901 208 5.75324 196 5.75746 218 5.76169 240 5.76591 256 5.77014 210 5.77437 224 5.77859 212 5.78282 215 5.78704 223 5.79127 189 5.79549 209 5.79972 175 5.80394 165 5.80817 187 5.81239 175 5.81662 184 5.82084 192 5.82507 199 5.8293 206 5.83352 188 5.83775 193 5.84197 164 5.8462 166 5.85042 156 5.85465 185 5.85887 216 5.8631 249 5.86732 337 5.87155 493 5.87577 702 5.87603 728 5.87603 508 5.87603 283 5.87603 134 5.87603 76 5.87603 50 5.87603 34 5.87603 45 5.87603 35 5.87603 92 5.87603 155 5.87603 177 5.87603 163 5.87603 161 5.87603 156 5.87603 148 5.87603 153 5.87603 190 5.87603 178 5.87603 129 5.87603 73 5.87603 41 5.87603 16 5.87603 10 5.87603 9 5.87603 7 5.87603 5 5.87603 2 5.87603 O 1s/2 nb_sba2.vms 2015 12 10 2 48 11 0 14 Casa Info Follows 2 Calib M = 281.846 A = 284.6 BE ADD Calib M = 284.648 A = 284.6 Regions Comps BE ADD 0 1 CASA region (*O 1s*) (*Shirley*) 943.936 963.936 0.78 2 0 0 299 542 275 9.3 (*O 1s*) 15.9994 0 2 CASA comp (*O 1s*) (*GL(30)*) Area 40789.443 0.001 10000000 -1 1 MFWHM 1.8757364 0.38 9.5 -1 1 Position 954.27988 943.936 963.936 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) CASA comp (*O 1s*) (*GL(30)*) Area 651.15835 0.001 10000000 -1 1 MFWHM 1.4288902 0.38 9.5 -1 1 Position 956.97341 943.936 963.936 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) nb_sba2.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 666 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 332 Charge Neutraliser :On Acquired On :15/12/10 02:48:11 XPS 54 5 1 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 O 1s -1 Kinetic Energy eV 946.69 0.1 2 Intensity d Transmission d pulse counting 0.3315 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 1938 69475 1.31473 1.31659 3924 1.31659 3877 1.31658 3789 1.31657 3702 1.31656 3486 1.31655 3403 1.31654 3330 1.31653 3277 1.31652 3260 1.31651 2981 1.3165 3033 1.3165 2976 1.31649 2963 1.31648 2862 1.31647 2857 1.31646 2775 1.31645 2680 1.31644 2541 1.31643 2600 1.31642 2581 1.31641 2569 1.3164 2504 1.31639 2516 1.31638 2560 1.31637 2462 1.31637 2472 1.31636 2493 1.31635 2447 1.31634 2367 1.31633 2504 1.31632 2365 1.31631 2450 1.3163 2351 1.31629 2426 1.31628 2383 1.31627 2438 1.31626 2436 1.31625 2414 1.31624 2355 1.31623 2424 1.31623 2424 1.31622 2328 1.31621 2410 1.3162 2432 1.31619 2383 1.31618 2395 1.31617 2330 1.31616 2318 1.31615 2342 1.31614 2366 1.31613 2321 1.31612 2331 1.31611 2326 1.3161 2320 1.3161 2322 1.31609 2318 1.31608 2353 1.31607 2370 1.31606 2350 1.31605 2317 1.31604 2329 1.31603 2274 1.31602 2304 1.31601 2396 1.316 2280 1.31599 2397 1.31598 2391 1.31597 2434 1.31597 2531 1.31596 2576 1.31595 2689 1.31594 2653 1.31593 2765 1.31592 2952 1.31591 3050 1.3159 3241 1.31589 3386 1.31588 3614 1.31587 4023 1.31586 4344 1.31585 4894 1.31584 5472 1.31584 6394 1.31583 7373 1.31582 8469 1.31581 9755 1.3158 11496 1.31579 13466 1.31578 15582 1.31577 18202 1.31576 21370 1.31575 24686 1.31574 28084 1.31573 32451 1.31572 36496 1.31571 41349 1.3157 45836 1.3157 50722 1.31569 54819 1.31568 59200 1.31567 62888 1.31566 65705 1.31565 67622 1.31564 69276 1.31563 69475 1.31562 68640 1.31561 66340 1.3156 62866 1.31559 59432 1.31558 54679 1.31557 49802 1.31557 44841 1.31556 39187 1.31555 34162 1.31554 29321 1.31553 25292 1.31552 21562 1.31551 17822 1.3155 15156 1.31549 12742 1.31548 10964 1.31547 9536 1.31546 8239 1.31545 7140 1.31544 6460 1.31544 5754 1.31543 5244 1.31542 4761 1.31541 4359 1.3154 4140 1.31539 3760 1.31538 3609 1.31537 3322 1.31536 3330 1.31535 3116 1.31534 2968 1.31533 2815 1.31532 2824 1.31531 2696 1.31531 2594 1.3153 2490 1.31529 2466 1.31528 2371 1.31527 2305 1.31526 2348 1.31525 2157 1.31524 2242 1.31523 2234 1.31522 2196 1.31521 2221 1.3152 2160 1.31519 2129 1.31518 2108 1.31517 2083 1.31517 2083 1.31516 2038 1.31515 2038 1.31514 2053 1.31513 2030 1.31512 1938 1.31511 2035 1.3151 2072 1.31509 2056 1.31508 1955 1.31507 2112 1.31506 2066 1.31505 2078 1.31504 1985 1.31504 2050 1.31503 2029 1.31502 1991 1.31501 1981 1.315 2016 1.31499 2017 1.31498 2048 1.31497 1997 1.31496 2027 1.31495 2018 1.31494 2002 1.31493 2024 1.31492 2008 1.31491 1979 1.31491 1987 1.3149 1955 1.31489 2065 1.31488 1979 1.31487 2005 1.31486 1992 1.31485 1938 1.31484 1977 1.31483 2000 1.31482 2024 1.31481 1967 1.3148 2012 1.31479 1995 1.31478 1946 1.31478 2005 1.31477 1999 1.31476 2020 1.31475 2060 1.31474 1941 1.31473 C 1s/3 nb_sba2.vms 2015 12 10 2 48 11 0 13 Casa Info Follows 2 Calib M = 281.846 A = 284.6 BE ADD Calib M = 284.648 A = 284.6 Regions Comps BE ADD 0 1 CASA region (*C 1s*) (*Shirley*) 1183.936 1213.936 0.278 2 0 0 299 542 275 9.3 (*C 1s*) 12.011 0 1 CASA comp (*C 1s*) (*GL(30)*) Area 310.89986 0.001 10000000 -1 1 MFWHM 2.1258382 0.34 8.5 -1 1 Position 1202.0006 1183.936 1213.936 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) nb_sba2.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 782 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 260 Charge Neutraliser :On Acquired On :15/12/10 02:48:11 XPS 54 5 1 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 C 1s -1 Kinetic Energy eV 1186.69 0.1 2 Intensity d Transmission d pulse counting 0.2597 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 602 1359 1921 1.23374 1.24606 1540 1.24606 1455 1.24602 1537 1.24598 1550 1.24594 1483 1.2459 1483 1.24586 1479 1.24581 1437 1.24577 1450 1.24573 1439 1.24569 1516 1.24565 1433 1.24561 1540 1.24557 1513 1.24553 1482 1.24549 1461 1.24544 1506 1.2454 1508 1.24536 1531 1.24532 1550 1.24528 1440 1.24524 1566 1.2452 1538 1.24516 1530 1.24512 1538 1.24507 1429 1.24503 1516 1.24499 1480 1.24495 1548 1.24491 1500 1.24487 1451 1.24483 1455 1.24479 1440 1.24475 1506 1.24471 1472 1.24466 1463 1.24462 1526 1.24458 1517 1.24454 1547 1.2445 1467 1.24446 1511 1.24442 1447 1.24438 1443 1.24434 1430 1.24429 1471 1.24425 1440 1.24421 1514 1.24417 1515 1.24413 1459 1.24409 1480 1.24405 1498 1.24401 1586 1.24397 1488 1.24392 1476 1.24388 1415 1.24384 1534 1.2438 1481 1.24376 1453 1.24372 1427 1.24368 1448 1.24364 1410 1.2436 1449 1.24355 1439 1.24351 1602 1.24347 1508 1.24343 1462 1.24339 1436 1.24335 1429 1.24331 1513 1.24327 1443 1.24323 1463 1.24319 1478 1.24314 1508 1.2431 1535 1.24306 1526 1.24302 1447 1.24298 1511 1.24294 1513 1.2429 1450 1.24286 1480 1.24282 1494 1.24277 1486 1.24273 1572 1.24269 1513 1.24265 1419 1.24261 1403 1.24257 1457 1.24253 1445 1.24249 1485 1.24245 1448 1.2424 1563 1.24236 1449 1.24232 1477 1.24228 1451 1.24224 1467 1.2422 1503 1.24216 1469 1.24212 1462 1.24208 1492 1.24203 1525 1.24199 1525 1.24195 1532 1.24191 1444 1.24187 1517 1.24183 1493 1.24179 1533 1.24175 1475 1.24171 1512 1.24167 1475 1.24162 1465 1.24158 1496 1.24154 1458 1.2415 1521 1.24146 1473 1.24142 1466 1.24138 1459 1.24134 1500 1.2413 1464 1.24125 1483 1.24121 1508 1.24117 1451 1.24113 1474 1.24109 1480 1.24105 1498 1.24101 1469 1.24097 1468 1.24093 1503 1.24088 1494 1.24084 1502 1.2408 1550 1.24076 1502 1.24072 1492 1.24068 1493 1.24064 1472 1.2406 1535 1.24056 1497 1.24051 1503 1.24047 1515 1.24043 1485 1.24039 1533 1.24035 1468 1.24031 1541 1.24027 1553 1.24023 1504 1.24019 1489 1.24015 1483 1.2401 1487 1.24006 1583 1.24002 1508 1.23998 1530 1.23994 1487 1.2399 1551 1.23986 1409 1.23982 1502 1.23978 1583 1.23973 1579 1.23969 1641 1.23965 1531 1.23961 1558 1.23957 1582 1.23953 1590 1.23949 1601 1.23945 1626 1.23941 1605 1.23936 1592 1.23932 1651 1.23928 1606 1.23924 1722 1.2392 1708 1.23916 1657 1.23912 1731 1.23908 1743 1.23904 1673 1.23899 1671 1.23895 1706 1.23891 1789 1.23887 1735 1.23883 1770 1.23879 1782 1.23875 1831 1.23871 1881 1.23867 1873 1.23863 1921 1.23858 1863 1.23854 1870 1.2385 1805 1.23846 1826 1.23842 1820 1.23838 1768 1.23834 1739 1.2383 1740 1.23826 1670 1.23821 1646 1.23817 1585 1.23813 1572 1.23809 1591 1.23805 1573 1.23801 1556 1.23797 1526 1.23793 1471 1.23789 1472 1.23784 1448 1.2378 1451 1.23776 1548 1.23772 1444 1.23768 1459 1.23764 1478 1.2376 1511 1.23756 1444 1.23752 1428 1.23747 1472 1.23743 1453 1.23739 1435 1.23735 1471 1.23731 1509 1.23727 1359 1.23723 1477 1.23719 1488 1.23715 1456 1.23711 1504 1.23706 1389 1.23702 1486 1.23698 1447 1.23694 1530 1.2369 1433 1.23686 1386 1.23682 1470 1.23678 1461 1.23674 1439 1.23669 1426 1.23665 1467 1.23661 1437 1.23657 1506 1.23653 1405 1.23649 1441 1.23645 1447 1.23641 1476 1.23637 1396 1.23632 1441 1.23628 1432 1.23624 1457 1.2362 1438 1.23616 1500 1.23612 1483 1.23608 1506 1.23604 1458 1.236 1425 1.23595 1406 1.23591 1459 1.23587 1464 1.23583 1482 1.23579 1463 1.23575 1492 1.23571 1589 1.23567 1421 1.23563 1467 1.23559 1462 1.23554 1499 1.2355 1509 1.23546 1446 1.23542 1500 1.23538 1436 1.23534 1490 1.2353 1513 1.23526 1413 1.23522 1515 1.23517 1444 1.23513 1510 1.23509 1491 1.23505 1510 1.23501 1482 1.23497 1467 1.23493 1494 1.23489 1449 1.23485 1480 1.2348 1481 1.23476 1445 1.23472 1445 1.23468 1429 1.23464 1461 1.2346 1423 1.23456 1461 1.23452 1432 1.23448 1434 1.23443 1492 1.23439 1491 1.23435 1490 1.23431 1443 1.23427 1509 1.23423 1463 1.23419 1479 1.23415 1505 1.23411 1508 1.23407 1370 1.23402 1422 1.23398 1487 1.23394 1443 1.2339 1500 1.23386 1503 1.23382 1500 1.23378 1481 1.23374 Nb 3d/4 nb_sba2.vms 2015 12 10 2 48 11 0 14 Casa Info Follows 2 Calib M = 281.846 A = 284.6 BE ADD Calib M = 284.648 A = 284.6 Regions Comps BE ADD 0 1 CASA region (*Nb 3d*) (*Shirley*) 1271.936 1283.5058 2.921 2 0 0 299 542 275 9.3 (*Nb 3d*) 92.9064 0 2 CASA comp (*Nb 3d*) (*GL(30)*) Area 785.43148 0.001 10000000 -1 1 MFWHM 2.1612209 0.56 14 -1 1 Position 1278.6691 1271.936 1288.936 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) CASA comp (*Nb 3d*) (*GL(30)*) Area 525.64198 0.001 10000000 -1 1 MFWHM 2.1498751 0.56 14 -1 1 Position 1275.885 1271.936 1288.936 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) nb_sba2.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 2350 Sweeps: 30 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 458 Charge Neutraliser :On Acquired On :15/12/10 02:48:11 XPS 54 5 1 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Nb 3d -1 Kinetic Energy eV 1274.69 0.1 2 Intensity d Transmission d pulse counting 0.458 30 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 342 7697 12500 1.20664 1.21249 7795 1.21249 7707 1.21245 7993 1.21242 8048 1.21239 7965 1.21235 8051 1.21232 7933 1.21228 7982 1.21225 8068 1.21221 7949 1.21218 7892 1.21214 7945 1.21211 8213 1.21208 8051 1.21204 8079 1.21201 7991 1.21197 7862 1.21194 7984 1.2119 8078 1.21187 8165 1.21183 8283 1.2118 8516 1.21177 8372 1.21173 8412 1.2117 8580 1.21166 8787 1.21163 8976 1.21159 8933 1.21156 9119 1.21152 9419 1.21149 9549 1.21146 9806 1.21142 9982 1.21139 10253 1.21135 10470 1.21132 10561 1.21128 10668 1.21125 10945 1.21121 11057 1.21118 10955 1.21115 11086 1.21111 10958 1.21108 11013 1.21104 10828 1.21101 10868 1.21097 10709 1.21094 10518 1.2109 10460 1.21087 10388 1.21084 10437 1.2108 10161 1.21077 10206 1.21073 10207 1.2107 10268 1.21066 10390 1.21063 10546 1.21059 10588 1.21056 10809 1.21053 10862 1.21049 11306 1.21046 11529 1.21042 11588 1.21039 11936 1.21035 12401 1.21032 12132 1.21029 12217 1.21025 12500 1.21022 12464 1.21018 12433 1.21015 12336 1.21011 12017 1.21008 12048 1.21004 11849 1.21001 11531 1.20998 11407 1.20994 11288 1.20991 10703 1.20987 10343 1.20984 10193 1.2098 10078 1.20977 9726 1.20973 9347 1.2097 9158 1.20967 8993 1.20963 8696 1.2096 8369 1.20956 8383 1.20953 8397 1.20949 8195 1.20946 8094 1.20942 8080 1.20939 8074 1.20936 7776 1.20932 7847 1.20929 7739 1.20925 7962 1.20922 7881 1.20918 7890 1.20915 7918 1.20911 7921 1.20908 7815 1.20905 7925 1.20901 7799 1.20898 7778 1.20894 7734 1.20891 7912 1.20887 7991 1.20884 7836 1.2088 7841 1.20877 7750 1.20874 7759 1.2087 7839 1.20867 7983 1.20863 7906 1.2086 7966 1.20856 7750 1.20853 7697 1.20849 7955 1.20846 7853 1.20843 7726 1.20839 7811 1.20836 7745 1.20832 7855 1.20829 7815 1.20825 7900 1.20822 7891 1.20819 7908 1.20815 7985 1.20812 7859 1.20808 7869 1.20805 7907 1.20801 7861 1.20798 7850 1.20794 7846 1.20791 7992 1.20788 7975 1.20784 7882 1.20781 7867 1.20777 8045 1.20774 7834 1.2077 7904 1.20767 7837 1.20763 8056 1.2076 8074 1.20757 7952 1.20753 7880 1.2075 8022 1.20746 8004 1.20743 7978 1.20739 7998 1.20736 8029 1.20732 7955 1.20729 8017 1.20726 7993 1.20722 8109 1.20719 8013 1.20715 7901 1.20712 7988 1.20708 7974 1.20705 8187 1.20701 7951 1.20698 8088 1.20695 8054 1.20691 8037 1.20688 8028 1.20684 8050 1.20681 8038 1.20677 8147 1.20674 7960 1.2067 8259 1.20667 8154 1.20664 Si 2p/5 nb_sba2.vms 2015 12 10 2 48 11 0 13 Casa Info Follows 2 Calib M = 281.846 A = 284.6 BE ADD Calib M = 284.648 A = 284.6 Regions Comps BE ADD 0 1 CASA region (*Si 2p*) (*Shirley*) 1373.936 1393.936 0.328 2 0 0 299 542 275 9.3 (*Si 2p*) 28.0858 0 1 CASA comp (*Si 2p*) (*GL(30)*) Area 6688.8794 0.001 10000000 -1 1 MFWHM 1.7842459 0.4 10 -1 1 Position 1383.5441 1373.936 1393.936 -1 1 RSF 0.328 MASS 28.0858 INDEX -1 (*Si 2p*) CONST (**) nb_sba2.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 799 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 397 Charge Neutraliser :On Acquired On :15/12/10 02:48:11 XPS 54 5 1 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Si 2p -1 Kinetic Energy eV 1376.69 0.1 2 Intensity d Transmission d pulse counting 0.3974 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 432 14179 1.19156 1.19218 711 1.19218 713 1.19218 661 1.19217 659 1.19217 666 1.19217 629 1.19216 644 1.19216 639 1.19216 576 1.19215 579 1.19215 577 1.19215 593 1.19214 601 1.19214 554 1.19214 566 1.19213 559 1.19213 543 1.19213 573 1.19213 517 1.19212 541 1.19212 514 1.19212 569 1.19211 569 1.19211 552 1.19211 557 1.1921 537 1.1921 553 1.1921 543 1.19209 572 1.19209 549 1.19209 543 1.19209 554 1.19208 562 1.19208 552 1.19208 523 1.19207 525 1.19207 544 1.19207 554 1.19206 564 1.19206 575 1.19206 592 1.19205 563 1.19205 529 1.19205 581 1.19205 525 1.19204 569 1.19204 557 1.19204 540 1.19203 550 1.19203 544 1.19203 541 1.19202 511 1.19202 525 1.19202 531 1.19201 509 1.19201 529 1.19201 553 1.19201 588 1.192 520 1.192 521 1.192 536 1.19199 531 1.19199 529 1.19199 545 1.19198 566 1.19198 567 1.19198 566 1.19197 621 1.19197 600 1.19197 677 1.19196 651 1.19196 769 1.19196 772 1.19196 863 1.19195 983 1.19195 1125 1.19195 1174 1.19194 1483 1.19194 1742 1.19194 2040 1.19193 2409 1.19193 2938 1.19193 3396 1.19192 3988 1.19192 4782 1.19192 5672 1.19192 6609 1.19191 7490 1.19191 8384 1.19191 9694 1.1919 10549 1.1919 11522 1.1919 12309 1.19189 13134 1.19189 13469 1.19189 13894 1.19188 14179 1.19188 14157 1.19188 14063 1.19188 13351 1.19187 12682 1.19187 11782 1.19187 10648 1.19186 9777 1.19186 8668 1.19186 7514 1.19185 6421 1.19185 5406 1.19185 4393 1.19184 3730 1.19184 3036 1.19184 2508 1.19184 1936 1.19183 1669 1.19183 1400 1.19183 1067 1.19182 930 1.19182 823 1.19182 733 1.19181 704 1.19181 599 1.19181 576 1.1918 509 1.1918 496 1.1918 515 1.1918 546 1.19179 520 1.19179 473 1.19179 496 1.19178 522 1.19178 490 1.19178 475 1.19177 488 1.19177 485 1.19177 457 1.19176 452 1.19176 489 1.19176 440 1.19176 453 1.19175 491 1.19175 480 1.19175 432 1.19174 435 1.19174 478 1.19174 476 1.19173 473 1.19173 488 1.19173 503 1.19172 453 1.19172 445 1.19172 472 1.19171 463 1.19171 473 1.19171 486 1.19171 498 1.1917 471 1.1917 462 1.1917 458 1.19169 489 1.19169 474 1.19169 468 1.19168 505 1.19168 510 1.19168 466 1.19167 461 1.19167 459 1.19167 458 1.19167 473 1.19166 479 1.19166 483 1.19166 504 1.19165 471 1.19165 449 1.19165 499 1.19164 451 1.19164 535 1.19164 472 1.19163 461 1.19163 474 1.19163 506 1.19163 476 1.19162 477 1.19162 473 1.19162 467 1.19161 507 1.19161 521 1.19161 508 1.1916 525 1.1916 432 1.1916 490 1.19159 479 1.19159 451 1.19159 482 1.19159 461 1.19158 460 1.19158 480 1.19158 458 1.19157 480 1.19157 438 1.19157 466 1.19156 482 1.19156 wide/1 nb_sba5.vms 2015 12 10 4 44 33 0 10 Casa Info Follows 1 Calib M = 282.697 A = 284.6 BE ADD 0 0 0 nb_sba5.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 160 Acqn. Time(s): 603 Sweeps: 5 Anode:Mono(Al (Mono))(156 W) Step(meV): 1000.0 Dwell Time(ms): 100 Charge Neutraliser :On Acquired On :15/12/10 04:44:33 XPS 54 0 2 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 160 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Wide None -1 Kinetic Energy eV 286.69 1 2 Intensity d Transmission d pulse counting 0.1 5 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 2412 1 25572 4.41569 8.42235 3036 8.42235 3127 8.38839 3121 8.35442 3090 8.32045 3085 8.28649 3118 8.25252 3117 8.21856 3202 8.18459 3041 8.15063 3081 8.11666 3068 8.0827 3035 8.04873 3077 8.01476 3145 7.9808 3090 7.94683 3148 7.91287 3053 7.8789 3181 7.84494 3139 7.81097 3134 7.77701 3120 7.74304 3120 7.70907 3163 7.67511 3191 7.64114 3126 7.60718 3233 7.57321 3134 7.53925 3169 7.50528 3220 7.47131 3107 7.43735 3195 7.40338 3211 7.36942 3092 7.33545 3198 7.30149 3271 7.26752 3176 7.23356 3252 7.19959 3216 7.16562 3247 7.13166 3247 7.09769 3219 7.06373 3242 7.02976 3268 7.00512 3242 6.99202 3268 6.97893 3228 6.96583 3150 6.95273 3197 6.93963 3168 6.92653 3169 6.91343 3228 6.90033 3181 6.88723 3199 6.87414 3325 6.86104 3267 6.84794 3298 6.83484 3287 6.82174 3260 6.80864 3357 6.79554 3335 6.78244 3373 6.76935 3383 6.75625 3307 6.74315 3306 6.73005 3355 6.71695 3355 6.70385 3375 6.69075 3280 6.67765 3302 6.66456 3261 6.65146 3359 6.63836 3389 6.62526 3370 6.61216 3412 6.59906 3355 6.58596 3412 6.57286 3345 6.55976 3307 6.54667 3363 6.53357 3381 6.52047 3470 6.50737 3417 6.49427 3317 6.48117 3434 6.46807 3422 6.45497 3451 6.44188 3417 6.42878 3407 6.41568 3451 6.40258 3472 6.38948 3411 6.37638 3455 6.36328 3537 6.35018 3462 6.33709 3537 6.32399 3525 6.31089 3590 6.29779 3554 6.28469 3493 6.27159 3523 6.25849 3597 6.24539 3588 6.2323 3554 6.2192 3561 6.2061 3606 6.193 3593 6.1799 3592 6.1668 3554 6.1537 3564 6.1406 3585 6.1275 3548 6.11441 3618 6.10131 3620 6.08821 3644 6.07511 3624 6.06201 3525 6.04891 3662 6.03581 3651 6.02271 3653 6.00962 3609 5.99652 3743 5.98342 3657 5.97032 3655 5.95722 3666 5.94412 3713 5.93102 3731 5.91792 3761 5.90483 3744 5.89173 3727 5.87863 3608 5.86553 3737 5.85243 3768 5.83933 3800 5.82623 3750 5.81313 3873 5.80004 3808 5.78694 3854 5.77384 3837 5.76074 3821 5.74764 3842 5.73454 3892 5.72144 3806 5.70834 3873 5.69524 3914 5.68215 3742 5.66905 3741 5.65595 3937 5.64285 3936 5.62975 3879 5.61665 3990 5.60355 3983 5.59045 3944 5.57736 4096 5.56426 4023 5.55116 3909 5.53806 4006 5.52496 4009 5.51186 3968 5.49876 4164 5.48566 4044 5.47257 4088 5.45947 4110 5.44637 4086 5.43327 4087 5.42017 3954 5.40707 4126 5.39397 4020 5.38087 4163 5.36778 4134 5.35468 4177 5.34158 4100 5.33457 4195 5.33071 4205 5.32684 4165 5.32297 4127 5.31911 4093 5.31524 4257 5.31137 4194 5.30751 4255 5.30364 4332 5.29978 4386 5.29591 4438 5.29204 4415 5.28818 4529 5.28431 4484 5.28044 4572 5.27658 4641 5.27271 4526 5.26885 4381 5.26498 4454 5.26111 4501 5.25725 4408 5.25338 4369 5.24951 4373 5.24565 4486 5.24178 4543 5.23792 4697 5.23405 4712 5.23018 4780 5.22632 4811 5.22245 4971 5.21858 5064 5.21472 5109 5.21085 5034 5.20699 4956 5.20312 4831 5.19925 4557 5.19539 4569 5.19152 4549 5.18765 4379 5.18379 4331 5.17992 4256 5.17606 4312 5.17219 4315 5.16832 4346 5.16446 4320 5.16059 4410 5.15672 4562 5.15286 4870 5.14899 5208 5.14513 5542 5.14126 5779 5.13739 6233 5.13353 6638 5.12966 6659 5.12579 6026 5.12193 5381 5.11806 4970 5.1142 4586 5.11033 4210 5.10646 3965 5.1026 3621 5.09873 3421 5.09486 3178 5.091 2958 5.08713 2919 5.08327 2732 5.0794 2706 5.07553 2611 5.07167 2623 5.0678 2533 5.06393 2569 5.06007 2537 5.0562 2586 5.05234 2613 5.04847 2482 5.0446 2535 5.04074 2407 5.03687 2539 5.033 2551 5.02914 2521 5.02527 2540 5.02141 2527 5.01754 2480 5.01367 2592 5.00981 2574 5.00594 2487 5.00207 2546 4.99821 2570 4.99434 2631 4.99048 2576 4.98661 2551 4.98274 2522 4.97888 2549 4.97501 2553 4.97114 2592 4.96728 2612 4.96341 2550 4.95955 2672 4.95568 2661 4.95181 2588 4.94795 2555 4.94408 2611 4.94021 2635 4.93635 2512 4.93248 2706 4.92862 2737 4.92475 2664 4.92088 2578 4.91702 2685 4.91315 2667 4.90928 2669 4.90542 2719 4.90155 2661 4.89769 2692 4.89382 2610 4.88995 2757 4.88609 2600 4.88222 2635 4.87835 2685 4.87449 2675 4.87062 2679 4.86676 2784 4.86289 2743 4.85902 2734 4.85516 2753 4.85129 2737 4.84742 2693 4.84356 2696 4.83969 2878 4.83582 2742 4.83196 2699 4.82809 2725 4.82423 2813 4.82036 2818 4.81649 2815 4.81263 2749 4.80876 2767 4.80489 2798 4.80103 2736 4.79716 2737 4.7933 2795 4.78943 2724 4.78556 2826 4.7817 2875 4.77783 2789 4.77396 2673 4.7701 2770 4.76623 2752 4.76237 2917 4.7585 2931 4.75463 2893 4.75077 2949 4.7469 2907 4.74303 2941 4.73917 2981 4.7353 2890 4.73144 2954 4.72757 3019 4.7237 2975 4.71984 2951 4.71597 2800 4.7121 2821 4.70824 2803 4.70437 2791 4.70051 2835 4.69664 2880 4.69277 2983 4.68891 3026 4.68504 3017 4.68117 2911 4.67731 2986 4.67344 2939 4.66958 2991 4.66571 3137 4.66184 3097 4.65798 3278 4.65411 3186 4.65024 3142 4.64638 3045 4.64251 2858 4.63865 2810 4.63478 2842 4.63091 2806 4.62705 2910 4.62318 2851 4.61931 2849 4.61545 2885 4.61158 2877 4.60772 2815 4.60385 2832 4.59998 2889 4.59612 2980 4.59225 2947 4.58838 2843 4.58452 2838 4.58065 2877 4.57679 2924 4.57292 2928 4.56905 2930 4.56519 2852 4.56132 2894 4.55745 2874 4.55359 2900 4.54972 2908 4.54586 2928 4.54199 2939 4.53812 2850 4.53426 2894 4.53039 3047 4.52906 3008 4.52854 2909 4.52803 2900 4.52752 2975 4.52701 3018 4.52649 2976 4.52598 2997 4.52547 2930 4.52495 3038 4.52444 3096 4.52393 3081 4.52341 3105 4.5229 3065 4.52239 3017 4.52188 2950 4.52136 3090 4.52085 3006 4.52034 2968 4.51982 3009 4.51931 2999 4.5188 3101 4.51828 3030 4.51777 3095 4.51726 3030 4.51675 3053 4.51623 3106 4.51572 3121 4.51521 3176 4.51469 3114 4.51418 3024 4.51367 3168 4.51315 3088 4.51264 3200 4.51213 3063 4.51162 3148 4.5111 3097 4.51059 3123 4.51008 3260 4.50956 3114 4.50905 3218 4.50854 3258 4.50803 3234 4.50751 3130 4.507 3228 4.50649 3205 4.50597 3267 4.50546 3199 4.50495 3187 4.50443 3209 4.50392 3310 4.50341 3239 4.50289 3279 4.50238 3183 4.50187 3080 4.50136 3220 4.50084 3128 4.50033 3211 4.49982 3226 4.4993 3125 4.49879 3179 4.49828 3255 4.49777 3259 4.49725 3168 4.49674 3210 4.49623 3176 4.49571 3167 4.4952 3245 4.49469 3214 4.49417 3261 4.49366 3324 4.49315 3269 4.49264 3365 4.49212 3288 4.49161 3243 4.4911 3316 4.49058 3321 4.49007 3369 4.48956 3317 4.48904 3244 4.48853 3328 4.48802 3351 4.48751 3262 4.48699 3389 4.48648 3311 4.48597 3287 4.48545 3406 4.48494 3345 4.48443 3299 4.48391 3288 4.4834 3292 4.48289 3417 4.48238 3453 4.48186 3330 4.48135 3280 4.48084 3333 4.48032 3282 4.47981 3368 4.4793 3408 4.47878 3365 4.47827 3402 4.47776 3498 4.47725 3422 4.47673 3473 4.47622 3406 4.47571 3409 4.47519 3484 4.47468 3551 4.47417 3641 4.47365 3466 4.47314 3448 4.47263 3472 4.47212 3540 4.4716 3529 4.47109 3482 4.47058 3496 4.47006 3527 4.46955 3521 4.46904 3656 4.46852 3580 4.46801 3561 4.4675 3539 4.46699 3515 4.46647 3473 4.46596 3515 4.46545 3540 4.46493 3504 4.46442 3369 4.46391 3490 4.46339 3724 4.46288 3586 4.46237 3706 4.46186 3538 4.46134 3538 4.46083 3566 4.46032 3515 4.4598 3541 4.45929 3503 4.45878 3555 4.45826 3625 4.45775 3636 4.45724 3648 4.45673 3569 4.45621 3613 4.4557 3578 4.45519 3708 4.45467 3696 4.45416 3600 4.45365 3643 4.45313 3708 4.45262 3610 4.45211 3639 4.4516 3614 4.45108 3702 4.45057 3860 4.45006 3818 4.44954 3803 4.44903 3754 4.44852 3739 4.448 3797 4.44749 3758 4.44698 3786 4.44647 3759 4.44595 3772 4.44544 3847 4.44493 3711 4.44441 3673 4.4439 3779 4.44339 3774 4.44287 3740 4.44236 3904 4.44185 3866 4.44134 3781 4.44082 3893 4.44031 3854 4.4398 3791 4.43928 3880 4.43877 3876 4.43826 3938 4.43775 3907 4.43723 3853 4.43672 3915 4.43621 3916 4.43569 3921 4.43518 3927 4.43467 3891 4.43415 3970 4.43364 3928 4.43313 3935 4.43262 3943 4.4321 3930 4.43159 3938 4.43108 4039 4.43056 3997 4.43005 4070 4.42954 3961 4.42902 3958 4.42851 3938 4.428 3977 4.42748 3952 4.42697 3998 4.42646 4055 4.42595 4008 4.42543 4050 4.42492 4081 4.42441 4012 4.42389 3997 4.42338 3995 4.42287 3989 4.42236 4131 4.42184 4061 4.42133 4025 4.42082 4036 4.4203 3991 4.41979 4044 4.41928 4116 4.41876 4041 4.41825 4093 4.41774 4117 4.41723 4001 4.41671 4133 4.4162 4039 4.41569 4196 4.41652 4234 4.41746 4131 4.41841 4146 4.41936 4195 4.4203 4120 4.42125 4229 4.4222 4120 4.42315 4065 4.42409 4212 4.42504 4258 4.42599 4291 4.42694 4206 4.42788 4258 4.42883 4287 4.42978 4341 4.43073 4335 4.43167 4273 4.43262 4278 4.43357 4413 4.43451 4372 4.43546 4295 4.43641 4399 4.43736 4402 4.4383 4429 4.43925 4430 4.4402 4359 4.44115 4284 4.44209 4311 4.44304 4485 4.44399 4398 4.44494 4301 4.44588 4215 4.44683 4178 4.44778 4164 4.44873 4089 4.44967 4132 4.45062 4164 4.45157 4270 4.45251 4431 4.45346 4628 4.45441 4633 4.45536 4786 4.4563 4877 4.45725 4840 4.4582 5107 4.45915 5240 4.46009 5247 4.46104 5087 4.46199 4937 4.46294 4642 4.46388 4306 4.46483 4119 4.46578 3964 4.46672 3871 4.46767 3675 4.46862 3531 4.46957 3310 4.47051 2964 4.47146 2660 4.47241 2139 4.47336 1922 4.4743 1720 4.47525 1679 4.4762 1606 4.47715 1632 4.47809 1945 4.47904 4903 4.47999 14507 4.48094 25572 4.48188 24785 4.48283 13217 4.48378 4868 4.48472 2129 4.48567 1567 4.48662 1408 4.48757 1431 4.48851 1442 4.48946 1315 4.49041 1396 4.49136 1372 4.4923 1377 4.49325 1359 4.4942 1379 4.49515 1344 4.49609 1359 4.49704 1364 4.49799 1354 4.49893 1347 4.49988 1358 4.50083 1383 4.50178 1349 4.50272 1368 4.50367 1349 4.50462 1365 4.50557 1419 4.50651 1419 4.50746 1341 4.50841 1321 4.50936 1351 4.5103 1342 4.51125 1344 4.5122 1383 4.51314 1406 4.51409 1439 4.51504 1406 4.51599 1458 4.51693 1431 4.51788 1357 4.51883 1342 4.51978 1368 4.52072 1386 4.52167 1408 4.52262 1418 4.52357 1435 4.52451 1397 4.52546 1347 4.52641 1387 4.52736 1362 4.5283 1342 4.52925 1363 4.5302 1431 4.53114 1351 4.53209 1375 4.53304 1428 4.53399 1476 4.53493 1396 4.53588 1447 4.53683 1492 4.53778 1501 4.53872 1441 4.53967 1495 4.54062 1474 4.54157 1456 4.54251 1453 4.54346 1414 4.54441 1390 4.54535 1407 4.5463 1440 4.54725 1429 4.5482 1440 4.54914 1487 4.55009 1354 4.55104 1412 4.55199 1431 4.55293 1447 4.55388 1444 4.55483 1423 4.55578 1391 4.55764 1418 4.5599 1375 4.56217 1430 4.56443 1463 4.56669 1446 4.56896 1381 4.57122 1434 4.57349 1423 4.57575 1463 4.57801 1422 4.58028 1392 4.58254 1451 4.58481 1416 4.58707 1408 4.58933 1410 4.5916 1403 4.59386 1453 4.59613 1453 4.59839 1422 4.60065 1434 4.60292 1376 4.60518 1450 4.60745 1424 4.60971 1400 4.61197 1450 4.61424 1426 4.6165 1460 4.61877 1511 4.62103 1487 4.62329 1505 4.62556 1446 4.62782 1392 4.63009 1417 4.63235 1525 4.63461 1474 4.63688 1498 4.63914 1488 4.64141 1541 4.64367 1510 4.64593 1490 4.6482 1462 4.65046 1461 4.65273 1495 4.65499 1528 4.65725 1434 4.65952 1502 4.66178 1507 4.66405 1526 4.66631 1515 4.66857 1533 4.67084 1567 4.6731 1638 4.67537 1615 4.67763 1535 4.67989 1550 4.68216 1517 4.68442 1493 4.68669 1465 4.68895 1501 4.69121 1506 4.69348 1475 4.69574 1496 4.69801 1482 4.70027 1463 4.70253 1425 4.7048 1493 4.70706 1537 4.70933 1559 4.71159 1534 4.71385 1704 4.71612 1768 4.71838 1930 4.72065 1908 4.72291 1720 4.72517 1556 4.72744 1487 4.7297 1484 4.73197 1432 4.73423 1419 4.73649 1437 4.73876 1408 4.74102 1454 4.74329 1463 4.74555 1498 4.74781 1592 4.75008 1722 4.75234 2108 4.75461 2149 4.75687 1890 4.75913 1624 4.7614 1483 4.76366 1432 4.76593 1396 4.76819 1351 4.77045 1385 4.77272 1329 4.77498 1321 4.77725 1407 4.77951 1326 4.78177 1317 4.78404 1336 4.7863 1342 4.78857 1370 4.79083 1313 4.79309 1309 4.79536 1425 4.79762 1357 4.79989 1360 4.80215 1327 4.80441 1355 4.80668 1323 4.80894 1389 4.81121 1378 4.81347 1368 4.81573 1342 4.818 1366 4.82026 1343 4.82253 1375 4.82479 1368 4.82705 1375 4.82932 1374 4.83158 1414 4.83385 1399 4.83611 1417 4.83837 1326 4.84064 1320 4.8429 1367 4.84517 1390 4.84743 1413 4.84969 1338 4.85196 1388 4.85422 1370 4.85648 1401 4.85875 1409 4.86101 1398 4.86328 1410 4.86554 1412 4.86781 1449 4.87007 1404 4.87233 1411 4.8746 1376 4.87686 1393 4.87913 1425 4.88139 1433 4.88365 1451 4.88592 1408 4.88818 1399 4.89044 1393 4.89271 1484 4.89497 1458 4.89724 1432 4.8995 1410 4.90176 1324 4.90403 1371 4.90629 1409 4.90856 1420 4.91082 1415 4.91308 1347 4.91535 1372 4.91761 1440 4.91988 1452 4.92214 1446 4.9244 1391 4.92667 1465 4.92893 1425 4.9312 1509 4.93346 1605 4.93572 1727 4.93799 1733 4.94025 1630 4.94252 1497 4.94478 1408 4.94704 1426 4.94931 1435 4.95157 1419 4.95384 1365 4.9561 1403 4.95836 1350 4.96063 1341 4.96289 1390 4.96516 1370 4.96742 1438 4.96968 1451 4.97195 1387 4.97421 1354 4.97648 1494 4.97874 1401 4.981 1413 4.98327 1427 4.98553 1430 4.9878 1403 4.99006 1444 4.99232 1428 4.99459 1438 4.99685 1493 4.99912 1394 5.00138 1391 5.00364 1499 5.00591 1473 5.00817 1479 5.01044 1448 5.01342 1436 5.01665 1499 5.01988 1527 5.02311 1467 5.02633 1441 5.02956 1434 5.03279 1405 5.03601 1518 5.03924 1401 5.04247 1510 5.0457 1504 5.04892 1514 5.05215 1449 5.05538 1452 5.05861 1519 5.06183 1459 5.06506 1547 5.06829 1481 5.07152 1551 5.07474 1555 5.07797 1568 5.0812 1605 5.08442 1609 5.08765 1573 5.09088 1586 5.09411 1564 5.09733 1560 5.10056 1577 5.10379 1588 5.10702 1549 5.11024 1596 5.11347 1567 5.1167 1491 5.11993 1509 5.12315 1476 5.12638 1464 5.12961 1416 5.13283 1408 5.13606 1552 5.13929 1564 5.14252 2014 5.14574 2333 5.14897 2468 5.1522 2621 5.15543 2674 5.15865 2222 5.16188 1635 5.16511 1359 5.16834 1406 5.17156 1393 5.17479 1349 5.17802 1442 5.18124 1414 5.18447 1457 5.1877 1388 5.19093 1401 5.19415 1383 5.19738 1394 5.20061 1378 5.20384 1389 5.20706 1403 5.21029 1410 5.21352 1376 5.21675 1397 5.21997 1403 5.2232 1451 5.22643 1440 5.22965 1433 5.23288 1449 5.23611 1438 5.23934 1454 5.24256 1459 5.24579 1528 5.24902 1564 5.25225 1593 5.25547 1571 5.2587 1630 5.26193 1618 5.26516 1670 5.26838 1529 5.27161 1575 5.27484 1522 5.27806 1507 5.28129 1452 5.28452 1331 5.28775 1252 5.29097 1251 5.2942 1208 5.29743 1077 5.30066 1046 5.30388 1002 5.30711 979 5.31034 1014 5.31381 1096 5.31803 1283 5.32226 1906 5.32648 3298 5.33071 5047 5.33493 5456 5.33916 4035 5.34338 2433 5.34761 1518 5.35183 1201 5.35606 1078 5.36028 1042 5.36451 983 5.36873 974 5.37296 967 5.37718 984 5.38141 926 5.38564 936 5.38986 915 5.39409 907 5.39831 926 5.40254 971 5.40676 926 5.41099 957 5.41521 889 5.41944 872 5.42366 870 5.42789 889 5.43211 924 5.43634 956 5.44056 990 5.44479 1072 5.44902 1054 5.45324 1069 5.45747 1043 5.46169 1148 5.46592 1113 5.47014 1038 5.47437 1023 5.47859 961 5.48282 1023 5.48704 881 5.49127 882 5.49549 762 5.49972 743 5.50394 638 5.50817 595 5.5124 468 5.51662 446 5.52085 416 5.52507 402 5.5293 416 5.53352 426 5.53775 853 5.54197 2446 5.5462 5216 5.55042 5967 5.55465 3591 5.55887 1208 5.5631 475 5.56732 376 5.57155 340 5.57578 357 5.58 374 5.58423 352 5.58845 343 5.59268 370 5.5969 354 5.60113 370 5.60535 381 5.60958 380 5.6138 375 5.61803 372 5.62225 364 5.62648 378 5.6307 374 5.63493 341 5.63916 370 5.64338 408 5.64761 390 5.65183 399 5.65606 409 5.66028 395 5.66451 399 5.66873 404 5.67296 413 5.67718 382 5.68141 396 5.68563 419 5.68986 416 5.69408 444 5.69831 429 5.70254 439 5.70676 413 5.71099 358 5.71521 391 5.71944 419 5.72366 412 5.72789 418 5.73211 405 5.73634 399 5.74056 331 5.74479 365 5.74901 354 5.75324 376 5.75746 375 5.76169 367 5.76591 395 5.77014 417 5.77437 403 5.77859 384 5.78282 415 5.78704 362 5.79127 364 5.79549 378 5.79972 362 5.80394 352 5.80817 310 5.81239 384 5.81662 361 5.82084 416 5.82507 455 5.8293 509 5.83352 466 5.83775 409 5.84197 317 5.8462 307 5.85042 305 5.85465 313 5.85887 339 5.8631 417 5.86732 593 5.87155 851 5.87577 1124 5.87603 1209 5.87603 911 5.87603 512 5.87603 290 5.87603 151 5.87603 94 5.87603 79 5.87603 60 5.87603 84 5.87603 165 5.87603 222 5.87603 260 5.87603 293 5.87603 279 5.87603 232 5.87603 244 5.87603 295 5.87603 326 5.87603 321 5.87603 255 5.87603 146 5.87603 74 5.87603 43 5.87603 31 5.87603 18 5.87603 4 5.87603 3 5.87603 1 5.87603 O 1s/2 nb_sba5.vms 2015 12 10 5 4 12 0 13 Casa Info Follows 1 Calib M = 281.864 A = 284.6 BE ADD 0 1 CASA region (*O 1s*) (*Shirley*) 943.954 963.954 0.78 2 0 0 299 542 275 9.3 (*O 1s*) 15.9994 0 2 CASA comp (*O 1s*) (*GL(30)*) Area 56350.647 0.001 10000000 -1 1 MFWHM 1.8152995 0.38 9.5 -1 1 Position 954.28769 943.954 963.954 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) CASA comp (*O 1s*) (*GL(30)*) Area 2324.4357 0.001 10000000 -1 1 MFWHM 1.7717395 0.37233596 9.3083989 -1 1 Position 956.53355 943.954 963.954 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) nb_sba5.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 666 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 332 Charge Neutraliser :On Acquired On :15/12/10 05:04:12 XPS 63 0 2 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 O 1s -1 Kinetic Energy eV 946.69 0.1 2 Intensity d Transmission d pulse counting 0.3315 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 3204 99920 1.31473 1.31659 6289 1.31659 6194 1.31658 5902 1.31657 5835 1.31656 5676 1.31655 5450 1.31654 5403 1.31653 5307 1.31652 5273 1.31651 5165 1.3165 5077 1.3165 4979 1.31649 4888 1.31648 4899 1.31647 4703 1.31646 4661 1.31645 4511 1.31644 4619 1.31643 4553 1.31642 4566 1.31641 4338 1.3164 4396 1.31639 4398 1.31638 4293 1.31637 4265 1.31637 4267 1.31636 4192 1.31635 4410 1.31634 4210 1.31633 4158 1.31632 4221 1.31631 4274 1.3163 4233 1.31629 4180 1.31628 4179 1.31627 4208 1.31626 4058 1.31625 4198 1.31624 4099 1.31623 4115 1.31623 4124 1.31622 4054 1.31621 4080 1.3162 3986 1.31619 4040 1.31618 4017 1.31617 4035 1.31616 4043 1.31615 3986 1.31614 3808 1.31613 3823 1.31612 3798 1.31611 3880 1.3161 3758 1.3161 3857 1.31609 3655 1.31608 3690 1.31607 3701 1.31606 3856 1.31605 3681 1.31604 3727 1.31603 3685 1.31602 3746 1.31601 3860 1.316 3826 1.31599 3943 1.31598 3963 1.31597 3913 1.31597 4044 1.31596 4013 1.31595 4202 1.31594 4163 1.31593 4434 1.31592 4622 1.31591 4818 1.3159 5175 1.31589 5512 1.31588 5683 1.31587 6075 1.31586 6665 1.31585 7373 1.31584 8041 1.31584 9127 1.31583 10263 1.31582 12050 1.31581 13542 1.3158 15874 1.31579 18485 1.31578 21611 1.31577 25042 1.31576 28972 1.31575 33712 1.31574 39114 1.31573 45254 1.31572 51499 1.31571 58174 1.3157 65017 1.3157 72295 1.31569 79200 1.31568 85022 1.31567 90285 1.31566 95186 1.31565 97887 1.31564 99920 1.31563 99528 1.31562 97689 1.31561 94742 1.3156 89364 1.31559 83908 1.31558 76791 1.31557 69191 1.31557 61564 1.31556 54127 1.31555 47402 1.31554 41047 1.31553 35332 1.31552 30180 1.31551 26270 1.3155 22963 1.31549 19858 1.31548 17565 1.31547 15715 1.31546 13871 1.31545 12601 1.31544 11366 1.31544 10416 1.31543 9523 1.31542 8709 1.31541 7923 1.3154 7401 1.31539 6790 1.31538 6323 1.31537 5996 1.31536 5608 1.31535 5486 1.31534 5323 1.31533 5192 1.31532 4850 1.31531 4549 1.31531 4511 1.3153 4406 1.31529 4234 1.31528 4091 1.31527 3862 1.31526 3860 1.31525 3751 1.31524 3642 1.31523 3715 1.31522 3594 1.31521 3565 1.3152 3492 1.31519 3488 1.31518 3474 1.31517 3476 1.31517 3399 1.31516 3417 1.31515 3342 1.31514 3286 1.31513 3404 1.31512 3328 1.31511 3329 1.3151 3335 1.31509 3331 1.31508 3233 1.31507 3409 1.31506 3299 1.31505 3297 1.31504 3318 1.31504 3292 1.31503 3265 1.31502 3273 1.31501 3327 1.315 3206 1.31499 3386 1.31498 3348 1.31497 3263 1.31496 3229 1.31495 3287 1.31494 3294 1.31493 3268 1.31492 3306 1.31491 3258 1.31491 3258 1.3149 3271 1.31489 3274 1.31488 3242 1.31487 3236 1.31486 3268 1.31485 3270 1.31484 3238 1.31483 3204 1.31482 3373 1.31481 3316 1.3148 3209 1.31479 3325 1.31478 3313 1.31478 3316 1.31477 3225 1.31476 3318 1.31475 3205 1.31474 3218 1.31473 C 1s/3 nb_sba5.vms 2015 12 10 5 4 12 0 13 Casa Info Follows 1 Calib M = 281.864 A = 284.6 BE ADD 0 1 CASA region (*C 1s*) (*Shirley*) 1183.954 1213.954 0.278 2 0 0 299 542 275 9.3 (*C 1s*) 12.011 0 2 CASA comp (*C 1s*) (*GL(30)*) Area 620.05695 0.001 10000000 -1 1 MFWHM 2.0410913 0.5 12.5 -1 1 Position 1201.9403 1183.954 1213.954 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) CASA comp (*C 1s*) (*GL(30)*) Area 332.9578 0.001 10000000 -1 1 MFWHM 3.6430373 0.53504031 13.376008 -1 1 Position 1199.8831 1183.954 1213.954 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) nb_sba5.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 782 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 260 Charge Neutraliser :On Acquired On :15/12/10 05:04:12 XPS 63 0 2 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 C 1s -1 Kinetic Energy eV 1186.69 0.1 2 Intensity d Transmission d pulse counting 0.2597 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 602 2228 3117 1.23374 1.24606 2340 1.24606 2343 1.24602 2369 1.24598 2391 1.24594 2405 1.2459 2316 1.24586 2362 1.24581 2357 1.24577 2355 1.24573 2348 1.24569 2388 1.24565 2388 1.24561 2393 1.24557 2347 1.24553 2411 1.24549 2409 1.24544 2337 1.2454 2382 1.24536 2367 1.24532 2400 1.24528 2322 1.24524 2361 1.2452 2444 1.24516 2371 1.24512 2423 1.24507 2343 1.24503 2336 1.24499 2378 1.24495 2444 1.24491 2396 1.24487 2283 1.24483 2359 1.24479 2294 1.24475 2297 1.24471 2244 1.24466 2337 1.24462 2376 1.24458 2314 1.24454 2401 1.2445 2382 1.24446 2401 1.24442 2379 1.24438 2356 1.24434 2349 1.24429 2301 1.24425 2414 1.24421 2314 1.24417 2269 1.24413 2305 1.24409 2320 1.24405 2380 1.24401 2278 1.24397 2382 1.24392 2355 1.24388 2415 1.24384 2425 1.2438 2290 1.24376 2433 1.24372 2361 1.24368 2409 1.24364 2389 1.2436 2300 1.24355 2305 1.24351 2320 1.24347 2379 1.24343 2358 1.24339 2388 1.24335 2323 1.24331 2329 1.24327 2329 1.24323 2400 1.24319 2307 1.24314 2401 1.2431 2373 1.24306 2304 1.24302 2453 1.24298 2332 1.24294 2274 1.2429 2403 1.24286 2335 1.24282 2350 1.24277 2390 1.24273 2297 1.24269 2480 1.24265 2241 1.24261 2265 1.24257 2295 1.24253 2429 1.24249 2394 1.24245 2323 1.2424 2308 1.24236 2312 1.24232 2335 1.24228 2264 1.24224 2392 1.2422 2377 1.24216 2356 1.24212 2384 1.24208 2367 1.24203 2263 1.24199 2330 1.24195 2386 1.24191 2458 1.24187 2329 1.24183 2308 1.24179 2299 1.24175 2346 1.24171 2292 1.24167 2263 1.24162 2373 1.24158 2324 1.24154 2331 1.2415 2386 1.24146 2327 1.24142 2295 1.24138 2340 1.24134 2324 1.2413 2327 1.24125 2353 1.24121 2367 1.24117 2378 1.24113 2323 1.24109 2406 1.24105 2425 1.24101 2385 1.24097 2304 1.24093 2340 1.24088 2394 1.24084 2350 1.2408 2374 1.24076 2411 1.24072 2435 1.24068 2370 1.24064 2419 1.2406 2449 1.24056 2423 1.24051 2514 1.24047 2420 1.24043 2378 1.24039 2576 1.24035 2402 1.24031 2410 1.24027 2480 1.24023 2409 1.24019 2499 1.24015 2445 1.2401 2476 1.24006 2547 1.24002 2530 1.23998 2447 1.23994 2481 1.2399 2513 1.23986 2530 1.23982 2534 1.23978 2387 1.23973 2559 1.23969 2584 1.23965 2619 1.23961 2519 1.23957 2694 1.23953 2558 1.23949 2642 1.23945 2743 1.23941 2680 1.23936 2757 1.23932 2684 1.23928 2774 1.23924 2800 1.2392 2909 1.23916 2845 1.23912 2931 1.23908 2933 1.23904 3005 1.23899 3018 1.23895 3018 1.23891 3037 1.23887 3081 1.23883 3098 1.23879 3104 1.23875 3107 1.23871 3077 1.23867 3095 1.23863 3084 1.23858 3071 1.23854 3056 1.2385 3052 1.23846 3117 1.23842 3034 1.23838 2911 1.23834 2828 1.2383 2686 1.23826 2622 1.23821 2707 1.23817 2568 1.23813 2461 1.23809 2513 1.23805 2473 1.23801 2440 1.23797 2286 1.23793 2327 1.23789 2329 1.23784 2287 1.2378 2318 1.23776 2280 1.23772 2359 1.23768 2262 1.23764 2272 1.2376 2344 1.23756 2273 1.23752 2299 1.23747 2313 1.23743 2332 1.23739 2272 1.23735 2333 1.23731 2312 1.23727 2265 1.23723 2376 1.23719 2385 1.23715 2295 1.23711 2361 1.23706 2232 1.23702 2298 1.23698 2288 1.23694 2312 1.2369 2337 1.23686 2335 1.23682 2315 1.23678 2324 1.23674 2392 1.23669 2296 1.23665 2293 1.23661 2412 1.23657 2370 1.23653 2299 1.23649 2294 1.23645 2238 1.23641 2326 1.23637 2318 1.23632 2254 1.23628 2381 1.23624 2377 1.2362 2279 1.23616 2367 1.23612 2297 1.23608 2308 1.23604 2367 1.236 2253 1.23595 2348 1.23591 2260 1.23587 2304 1.23583 2260 1.23579 2316 1.23575 2361 1.23571 2228 1.23567 2361 1.23563 2396 1.23559 2284 1.23554 2287 1.2355 2378 1.23546 2282 1.23542 2347 1.23538 2353 1.23534 2354 1.2353 2321 1.23526 2265 1.23522 2340 1.23517 2354 1.23513 2298 1.23509 2340 1.23505 2391 1.23501 2436 1.23497 2372 1.23493 2319 1.23489 2313 1.23485 2334 1.2348 2273 1.23476 2301 1.23472 2345 1.23468 2291 1.23464 2334 1.2346 2409 1.23456 2294 1.23452 2369 1.23448 2301 1.23443 2359 1.23439 2392 1.23435 2393 1.23431 2393 1.23427 2402 1.23423 2345 1.23419 2343 1.23415 2359 1.23411 2316 1.23407 2407 1.23402 2356 1.23398 2318 1.23394 2344 1.2339 2312 1.23386 2348 1.23382 2347 1.23378 2329 1.23374 Nb 3d/4 nb_sba5.vms 2015 12 10 5 4 12 0 13 Casa Info Follows 1 Calib M = 281.864 A = 284.6 Regions Comps BE ADD 0 1 CASA region (*Nb 3d*) (*Shirley*) 1274.69 1285.8778 2.921 2 0 0 299 542 275 9.3 (*Nb 3d*) 92.9064 0 2 CASA comp (*Nb 3d*) (*GL(30)*) Area 2392.2715 0.001 10000000 -1 1 MFWHM 2.0339978 0.48 12 -1 1 Position 1281.4928 1274.69 1291.69 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) CASA comp (*Nb 3d*) (*GL(30)*) Area 1556.6877 0.001 10000000 -1 1 MFWHM 2.0058325 0.48 12 -1 1 Position 1278.7454 1274.69 1291.69 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) nb_sba5.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 2350 Sweeps: 30 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 458 Charge Neutraliser :On Acquired On :15/12/10 05:04:12 XPS 63 0 2 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Nb 3d -1 Kinetic Energy eV 1274.69 0.1 2 Intensity d Transmission d pulse counting 0.458 30 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 342 11335 26772 1.20664 1.21249 12324 1.21249 12350 1.21245 12380 1.21242 12032 1.21239 12277 1.21235 12272 1.21232 12344 1.21228 12081 1.21225 12144 1.21221 12187 1.21218 12172 1.21214 12135 1.21211 12183 1.21208 12336 1.21204 12478 1.21201 12435 1.21197 12280 1.21194 12348 1.2119 12691 1.21187 12631 1.21183 12721 1.2118 12983 1.21177 13278 1.21173 13439 1.2117 13869 1.21166 14169 1.21163 14919 1.21159 15376 1.21156 15619 1.21152 16390 1.21149 17143 1.21146 17277 1.21142 18319 1.21139 19123 1.21135 19561 1.21132 20160 1.21128 20828 1.21125 21224 1.21121 21727 1.21118 21992 1.21115 22131 1.21111 21941 1.21108 22157 1.21104 21594 1.21101 21631 1.21097 21311 1.21094 20935 1.2109 20468 1.21087 19843 1.21084 19979 1.2108 19347 1.21077 18784 1.21073 19024 1.2107 19065 1.21066 19123 1.21063 19461 1.21059 19831 1.21056 20218 1.21053 20972 1.21049 21685 1.21046 22726 1.21042 23255 1.21039 23992 1.21035 24755 1.21032 25447 1.21029 26157 1.21025 26424 1.21022 26772 1.21018 26463 1.21015 26565 1.21011 26260 1.21008 25568 1.21004 25281 1.21001 24740 1.20998 23252 1.20994 22447 1.20991 21276 1.20987 20314 1.20984 19631 1.2098 18603 1.20977 17077 1.20973 16423 1.2097 15792 1.20967 15129 1.20963 14337 1.2096 13887 1.20956 13568 1.20953 13049 1.20949 12606 1.20946 12326 1.20942 12231 1.20939 12107 1.20936 11804 1.20932 11850 1.20929 11897 1.20925 11652 1.20922 11491 1.20918 11650 1.20915 11547 1.20911 11470 1.20908 11756 1.20905 11572 1.20901 11479 1.20898 11738 1.20894 11462 1.20891 11669 1.20887 11434 1.20884 11415 1.2088 11335 1.20877 11461 1.20874 11662 1.2087 11561 1.20867 11433 1.20863 11563 1.2086 11550 1.20856 11459 1.20853 11682 1.20849 11527 1.20846 11698 1.20843 11635 1.20839 11503 1.20836 11507 1.20832 11475 1.20829 11647 1.20825 11447 1.20822 11674 1.20819 11466 1.20815 11460 1.20812 11603 1.20808 11701 1.20805 11736 1.20801 11693 1.20798 11595 1.20794 11688 1.20791 11598 1.20788 11550 1.20784 11590 1.20781 11619 1.20777 11661 1.20774 11394 1.2077 11568 1.20767 11785 1.20763 11618 1.2076 11804 1.20757 11674 1.20753 11760 1.2075 11577 1.20746 11727 1.20743 11929 1.20739 11664 1.20736 11699 1.20732 11673 1.20729 11687 1.20726 11658 1.20722 11921 1.20719 11829 1.20715 11623 1.20712 11627 1.20708 11927 1.20705 11446 1.20701 11672 1.20698 11830 1.20695 11626 1.20691 11823 1.20688 11743 1.20684 11771 1.20681 11572 1.20677 11911 1.20674 11642 1.2067 11650 1.20667 11816 1.20664 Si 2p/5 nb_sba5.vms 2015 12 10 5 4 12 0 12 Casa Info Follows 1 Calib M = 281.864 A = 284.6 Regions Comps BE ADD 0 1 CASA region (*Si 2p*) (*Shirley*) 1376.69 1396.69 0.328 2 0 0 299 542 275 9.3 (*Si 2p*) 28.0858 0 1 CASA comp (*Si 2p*) (*GL(30)*) Area 9531.9682 0.001 10000000 -1 1 MFWHM 1.7656527 0.38 9.5 -1 1 Position 1386.3053 1376.69 1396.69 -1 1 RSF 0.328 MASS 28.0858 INDEX -1 (*Si 2p*) CONST (**) nb_sba5.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 799 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 397 Charge Neutraliser :On Acquired On :15/12/10 05:04:12 XPS 63 0 2 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Si 2p -1 Kinetic Energy eV 1376.69 0.1 2 Intensity d Transmission d pulse counting 0.3974 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 745 20813 1.19156 1.19218 1240 1.19218 1220 1.19218 1237 1.19217 1181 1.19217 1185 1.19217 1153 1.19216 1105 1.19216 1095 1.19216 1085 1.19215 1082 1.19215 1014 1.19215 1060 1.19214 1084 1.19214 1017 1.19214 987 1.19213 969 1.19213 970 1.19213 1017 1.19213 972 1.19212 947 1.19212 948 1.19212 970 1.19211 950 1.19211 957 1.19211 938 1.1921 993 1.1921 946 1.1921 876 1.19209 938 1.19209 928 1.19209 1036 1.19209 966 1.19208 953 1.19208 896 1.19208 935 1.19207 887 1.19207 942 1.19207 910 1.19206 886 1.19206 845 1.19206 947 1.19205 872 1.19205 874 1.19205 921 1.19205 863 1.19204 847 1.19204 876 1.19204 793 1.19203 890 1.19203 853 1.19203 807 1.19202 869 1.19202 840 1.19202 869 1.19201 884 1.19201 855 1.19201 816 1.19201 827 1.192 910 1.192 879 1.192 911 1.19199 927 1.19199 988 1.19199 1026 1.19198 976 1.19198 1026 1.19198 1097 1.19197 1132 1.19197 1140 1.19197 1234 1.19196 1293 1.19196 1408 1.19196 1450 1.19196 1667 1.19195 1757 1.19195 1937 1.19195 2218 1.19194 2462 1.19194 2761 1.19194 3159 1.19193 3754 1.19193 4503 1.19193 5393 1.19192 6110 1.19192 6995 1.19192 8098 1.19192 9393 1.19191 10621 1.19191 12033 1.19191 13450 1.1919 15131 1.1919 16407 1.1919 17703 1.19189 18564 1.19189 19334 1.19189 20450 1.19188 20716 1.19188 20813 1.19188 20156 1.19188 19581 1.19187 18587 1.19187 17372 1.19187 15804 1.19186 14225 1.19186 12495 1.19186 10840 1.19185 9105 1.19185 7605 1.19185 6357 1.19184 5231 1.19184 4330 1.19184 3335 1.19184 2833 1.19183 2296 1.19183 1906 1.19183 1584 1.19182 1384 1.19182 1232 1.19182 1163 1.19181 1024 1.19181 998 1.19181 849 1.1918 896 1.1918 844 1.1918 854 1.1918 864 1.19179 846 1.19179 866 1.19179 909 1.19178 888 1.19178 821 1.19178 789 1.19177 782 1.19177 811 1.19177 831 1.19176 797 1.19176 822 1.19176 838 1.19176 773 1.19175 833 1.19175 880 1.19175 824 1.19174 822 1.19174 805 1.19174 817 1.19173 810 1.19173 790 1.19173 745 1.19172 821 1.19172 816 1.19172 844 1.19171 883 1.19171 821 1.19171 850 1.19171 762 1.1917 839 1.1917 809 1.1917 862 1.19169 785 1.19169 854 1.19169 807 1.19168 806 1.19168 814 1.19168 784 1.19167 764 1.19167 826 1.19167 830 1.19167 821 1.19166 809 1.19166 823 1.19166 923 1.19165 810 1.19165 814 1.19165 839 1.19164 792 1.19164 787 1.19164 777 1.19163 792 1.19163 816 1.19163 827 1.19163 827 1.19162 815 1.19162 776 1.19162 790 1.19161 879 1.19161 804 1.19161 849 1.1916 809 1.1916 840 1.1916 828 1.19159 800 1.19159 791 1.19159 800 1.19159 782 1.19158 815 1.19158 821 1.19158 792 1.19157 809 1.19157 882 1.19157 837 1.19156 799 1.19156 wide/1 pnb.vms 2015 10 14 9 21 56 0 10 Casa Info Follows 1 Calib M = 281.048 A = 284.6 BE ADD 0 0 0 pnb.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 160 Acqn. Time(s): 603 Sweeps: 5 Anode:Mono(Al (Mono))(156 W) Step(meV): 1000.0 Dwell Time(ms): 100 Charge Neutraliser :On Acquired On :15/10/14 09:21:56 XPS 29 8 3 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 160 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Wide None -1 Kinetic Energy eV 286.69 1 2 Intensity d Transmission d pulse counting 0.1 5 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 2412 1 1577 4.41569 8.42235 364 8.42235 337 8.38839 367 8.35442 343 8.32045 328 8.28649 326 8.25252 334 8.21856 336 8.18459 339 8.15063 342 8.11666 310 8.0827 325 8.04873 343 8.01476 320 7.9808 322 7.94683 306 7.91287 346 7.8789 315 7.84494 339 7.81097 352 7.77701 335 7.74304 318 7.70907 363 7.67511 354 7.64114 340 7.60718 314 7.57321 327 7.53925 345 7.50528 367 7.47131 361 7.43735 321 7.40338 373 7.36942 352 7.33545 337 7.30149 337 7.26752 322 7.23356 334 7.19959 337 7.16562 338 7.13166 345 7.09769 363 7.06373 345 7.02976 350 7.00512 343 6.99202 318 6.97893 345 6.96583 340 6.95273 359 6.93963 350 6.92653 321 6.91343 330 6.90033 346 6.88723 360 6.87414 365 6.86104 340 6.84794 316 6.83484 323 6.82174 325 6.80864 380 6.79554 335 6.78244 357 6.76935 352 6.75625 348 6.74315 357 6.73005 327 6.71695 311 6.70385 346 6.69075 359 6.67765 377 6.66456 347 6.65146 335 6.63836 313 6.62526 336 6.61216 337 6.59906 360 6.58596 353 6.57286 328 6.55976 371 6.54667 322 6.53357 370 6.52047 335 6.50737 325 6.49427 337 6.48117 333 6.46807 340 6.45497 341 6.44188 342 6.42878 353 6.41568 344 6.40258 393 6.38948 380 6.37638 359 6.36328 353 6.35018 343 6.33709 351 6.32399 362 6.31089 353 6.29779 360 6.28469 357 6.27159 349 6.25849 346 6.24539 387 6.2323 385 6.2192 368 6.2061 361 6.193 346 6.1799 365 6.1668 379 6.1537 336 6.1406 378 6.1275 349 6.11441 354 6.10131 361 6.08821 365 6.07511 363 6.06201 357 6.04891 344 6.03581 347 6.02271 373 6.00962 335 5.99652 374 5.98342 349 5.97032 347 5.95722 360 5.94412 362 5.93102 391 5.91792 367 5.90483 367 5.89173 356 5.87863 384 5.86553 401 5.85243 387 5.83933 407 5.82623 384 5.81313 362 5.80004 335 5.78694 383 5.77384 370 5.76074 361 5.74764 377 5.73454 345 5.72144 388 5.70834 412 5.69524 397 5.68215 348 5.66905 345 5.65595 399 5.64285 387 5.62975 396 5.61665 398 5.60355 373 5.59045 399 5.57736 405 5.56426 403 5.55116 393 5.53806 416 5.52496 390 5.51186 387 5.49876 424 5.48566 429 5.47257 401 5.45947 375 5.44637 388 5.43327 379 5.42017 394 5.40707 364 5.39397 406 5.38087 412 5.36778 391 5.35468 363 5.34158 381 5.33457 385 5.33071 371 5.32684 389 5.32297 424 5.31911 413 5.31524 394 5.31137 418 5.30751 397 5.30364 380 5.29978 418 5.29591 409 5.29204 404 5.28818 415 5.28431 382 5.28044 419 5.27658 396 5.27271 430 5.26885 424 5.26498 383 5.26111 417 5.25725 429 5.25338 431 5.24951 430 5.24565 422 5.24178 418 5.23792 405 5.23405 431 5.23018 452 5.22632 435 5.22245 477 5.21858 426 5.21472 429 5.21085 433 5.20699 438 5.20312 426 5.19925 455 5.19539 487 5.19152 448 5.18765 448 5.18379 431 5.17992 439 5.17606 448 5.17219 460 5.16832 452 5.16446 421 5.16059 417 5.15672 423 5.15286 407 5.14899 400 5.14513 395 5.14126 410 5.13739 408 5.13353 420 5.12966 412 5.12579 472 5.12193 473 5.11806 522 5.1142 544 5.11033 557 5.10646 536 5.1026 481 5.09873 445 5.09486 434 5.091 417 5.08713 406 5.08327 363 5.0794 370 5.07553 388 5.07167 332 5.0678 361 5.06393 317 5.06007 326 5.0562 336 5.05234 332 5.04847 330 5.0446 323 5.04074 318 5.03687 356 5.033 300 5.02914 347 5.02527 346 5.02141 328 5.01754 333 5.01367 321 5.00981 335 5.00594 318 5.00207 323 4.99821 345 4.99434 354 4.99048 326 4.98661 325 4.98274 318 4.97888 348 4.97501 353 4.97114 338 4.96728 340 4.96341 349 4.95955 337 4.95568 341 4.95181 355 4.94795 348 4.94408 370 4.94021 339 4.93635 362 4.93248 338 4.92862 354 4.92475 342 4.92088 324 4.91702 342 4.91315 333 4.90928 331 4.90542 355 4.90155 335 4.89769 342 4.89382 356 4.88995 337 4.88609 369 4.88222 328 4.87835 346 4.87449 358 4.87062 338 4.86676 339 4.86289 333 4.85902 342 4.85516 341 4.85129 377 4.84742 344 4.84356 338 4.83969 339 4.83582 364 4.83196 355 4.82809 328 4.82423 336 4.82036 359 4.81649 369 4.81263 341 4.80876 326 4.80489 354 4.80103 355 4.79716 399 4.7933 407 4.78943 375 4.78556 367 4.7817 365 4.77783 338 4.77396 375 4.7701 366 4.76623 361 4.76237 374 4.7585 380 4.75463 380 4.75077 366 4.7469 368 4.74303 391 4.73917 369 4.7353 367 4.73144 350 4.72757 376 4.7237 355 4.71984 336 4.71597 362 4.7121 379 4.70824 383 4.70437 364 4.70051 382 4.69664 358 4.69277 363 4.68891 372 4.68504 357 4.68117 359 4.67731 417 4.67344 413 4.66958 372 4.66571 351 4.66184 378 4.65798 372 4.65411 378 4.65024 399 4.64638 364 4.64251 345 4.63865 356 4.63478 353 4.63091 352 4.62705 363 4.62318 346 4.61931 391 4.61545 392 4.61158 369 4.60772 383 4.60385 393 4.59998 408 4.59612 388 4.59225 389 4.58838 356 4.58452 394 4.58065 418 4.57679 390 4.57292 397 4.56905 377 4.56519 351 4.56132 400 4.55745 375 4.55359 384 4.54972 379 4.54586 398 4.54199 375 4.53812 388 4.53426 383 4.53039 397 4.52906 401 4.52854 373 4.52803 390 4.52752 377 4.52701 395 4.52649 423 4.52598 393 4.52547 370 4.52495 402 4.52444 404 4.52393 395 4.52341 370 4.5229 400 4.52239 415 4.52188 432 4.52136 408 4.52085 420 4.52034 392 4.51982 411 4.51931 403 4.5188 423 4.51828 434 4.51777 389 4.51726 400 4.51675 431 4.51623 475 4.51572 409 4.51521 405 4.51469 412 4.51418 402 4.51367 427 4.51315 430 4.51264 426 4.51213 444 4.51162 433 4.5111 412 4.51059 415 4.51008 413 4.50956 402 4.50905 420 4.50854 418 4.50803 401 4.50751 396 4.507 411 4.50649 440 4.50597 466 4.50546 427 4.50495 417 4.50443 401 4.50392 420 4.50341 441 4.50289 421 4.50238 454 4.50187 434 4.50136 437 4.50084 409 4.50033 408 4.49982 450 4.4993 453 4.49879 413 4.49828 438 4.49777 454 4.49725 403 4.49674 408 4.49623 415 4.49571 465 4.4952 429 4.49469 436 4.49417 468 4.49366 431 4.49315 495 4.49264 496 4.49212 451 4.49161 420 4.4911 427 4.49058 402 4.49007 464 4.48956 460 4.48904 468 4.48853 476 4.48802 445 4.48751 489 4.48699 439 4.48648 468 4.48597 482 4.48545 435 4.48494 405 4.48443 473 4.48391 459 4.4834 452 4.48289 491 4.48238 453 4.48186 460 4.48135 478 4.48084 463 4.48032 471 4.47981 471 4.4793 482 4.47878 437 4.47827 475 4.47776 499 4.47725 458 4.47673 468 4.47622 508 4.47571 458 4.47519 507 4.47468 460 4.47417 443 4.47365 450 4.47314 446 4.47263 473 4.47212 450 4.4716 491 4.47109 476 4.47058 486 4.47006 473 4.46955 466 4.46904 483 4.46852 478 4.46801 467 4.4675 446 4.46699 467 4.46647 539 4.46596 486 4.46545 501 4.46493 478 4.46442 457 4.46391 457 4.46339 457 4.46288 492 4.46237 445 4.46186 476 4.46134 445 4.46083 474 4.46032 477 4.4598 467 4.45929 478 4.45878 518 4.45826 517 4.45775 501 4.45724 499 4.45673 498 4.45621 483 4.4557 465 4.45519 527 4.45467 524 4.45416 455 4.45365 493 4.45313 484 4.45262 512 4.45211 498 4.4516 489 4.45108 495 4.45057 504 4.45006 502 4.44954 534 4.44903 520 4.44852 510 4.448 548 4.44749 506 4.44698 503 4.44647 513 4.44595 521 4.44544 487 4.44493 504 4.44441 521 4.4439 505 4.44339 525 4.44287 506 4.44236 513 4.44185 523 4.44134 520 4.44082 562 4.44031 529 4.4398 508 4.43928 543 4.43877 534 4.43826 496 4.43775 504 4.43723 528 4.43672 534 4.43621 520 4.43569 568 4.43518 532 4.43467 594 4.43415 530 4.43364 512 4.43313 518 4.43262 510 4.4321 549 4.43159 547 4.43108 545 4.43056 507 4.43005 534 4.42954 532 4.42902 548 4.42851 565 4.428 528 4.42748 559 4.42697 581 4.42646 556 4.42595 563 4.42543 556 4.42492 529 4.42441 495 4.42389 574 4.42338 560 4.42287 554 4.42236 536 4.42184 556 4.42133 570 4.42082 497 4.4203 527 4.41979 568 4.41928 617 4.41876 537 4.41825 547 4.41774 553 4.41723 582 4.41671 599 4.4162 552 4.41569 573 4.41652 618 4.41746 559 4.41841 568 4.41936 552 4.4203 613 4.42125 554 4.4222 566 4.42315 588 4.42409 595 4.42504 556 4.42599 593 4.42694 585 4.42788 606 4.42883 596 4.42978 580 4.43073 566 4.43167 565 4.43262 593 4.43357 545 4.43451 606 4.43546 580 4.43641 571 4.43736 575 4.4383 605 4.43925 608 4.4402 597 4.44115 614 4.44209 590 4.44304 576 4.44399 605 4.44494 591 4.44588 598 4.44683 594 4.44778 601 4.44873 586 4.44967 578 4.45062 591 4.45157 595 4.45251 612 4.45346 566 4.45441 631 4.45536 617 4.4563 600 4.45725 647 4.4582 609 4.45915 614 4.46009 605 4.46104 611 4.46199 629 4.46294 609 4.46388 592 4.46483 587 4.46578 588 4.46672 625 4.46767 619 4.46862 637 4.46957 632 4.47051 635 4.47146 639 4.47241 620 4.47336 575 4.4743 578 4.47525 552 4.4762 543 4.47715 532 4.47809 490 4.47904 536 4.47999 514 4.48094 589 4.48188 791 4.48283 1135 4.48378 1577 4.48472 1484 4.48567 923 4.48662 567 4.48757 478 4.48851 458 4.48946 473 4.49041 447 4.49136 476 4.4923 462 4.49325 485 4.4942 476 4.49515 484 4.49609 441 4.49704 441 4.49799 484 4.49893 469 4.49988 463 4.50083 476 4.50178 475 4.50272 477 4.50367 463 4.50462 478 4.50557 473 4.50651 491 4.50746 474 4.50841 484 4.50936 508 4.5103 503 4.51125 487 4.5122 483 4.51314 500 4.51409 504 4.51504 494 4.51599 447 4.51693 470 4.51788 476 4.51883 521 4.51978 490 4.52072 548 4.52167 478 4.52262 469 4.52357 526 4.52451 505 4.52546 500 4.52641 489 4.52736 488 4.5283 509 4.52925 489 4.5302 491 4.53114 492 4.53209 475 4.53304 511 4.53399 515 4.53493 520 4.53588 462 4.53683 515 4.53778 506 4.53872 546 4.53967 562 4.54062 554 4.54157 578 4.54251 578 4.54346 546 4.54441 521 4.54535 498 4.5463 490 4.54725 491 4.5482 472 4.54914 492 4.55009 526 4.55104 510 4.55199 479 4.55293 474 4.55388 463 4.55483 482 4.55578 487 4.55764 434 4.5599 451 4.56217 489 4.56443 454 4.56669 463 4.56896 511 4.57122 512 4.57349 473 4.57575 489 4.57801 466 4.58028 490 4.58254 483 4.58481 461 4.58707 467 4.58933 491 4.5916 505 4.59386 512 4.59613 508 4.59839 492 4.60065 513 4.60292 485 4.60518 498 4.60745 491 4.60971 470 4.61197 494 4.61424 514 4.6165 489 4.61877 497 4.62103 528 4.62329 527 4.62556 476 4.62782 490 4.63009 505 4.63235 494 4.63461 484 4.63688 504 4.63914 503 4.64141 516 4.64367 529 4.64593 508 4.6482 500 4.65046 517 4.65273 515 4.65499 516 4.65725 538 4.65952 542 4.66178 524 4.66405 500 4.66631 496 4.66857 501 4.67084 513 4.6731 524 4.67537 516 4.67763 512 4.67989 540 4.68216 526 4.68442 550 4.68669 507 4.68895 554 4.69121 564 4.69348 606 4.69574 519 4.69801 481 4.70027 519 4.70253 499 4.7048 512 4.70706 547 4.70933 549 4.71159 517 4.71385 527 4.71612 518 4.71838 621 4.72065 759 4.72291 863 4.72517 781 4.72744 645 4.7297 570 4.73197 525 4.73423 460 4.73649 444 4.73876 455 4.74102 469 4.74329 442 4.74555 428 4.74781 443 4.75008 507 4.75234 590 4.75461 831 4.75687 1013 4.75913 961 4.7614 764 4.76366 527 4.76593 407 4.76819 353 4.77045 371 4.77272 367 4.77498 334 4.77725 329 4.77951 353 4.78177 325 4.78404 304 4.7863 325 4.78857 313 4.79083 318 4.79309 309 4.79536 330 4.79762 319 4.79989 337 4.80215 327 4.80441 338 4.80668 350 4.80894 306 4.81121 327 4.81347 333 4.81573 330 4.818 333 4.82026 328 4.82253 341 4.82479 352 4.82705 322 4.82932 308 4.83158 346 4.83385 330 4.83611 341 4.83837 348 4.84064 318 4.8429 329 4.84517 332 4.84743 314 4.84969 316 4.85196 330 4.85422 358 4.85648 324 4.85875 364 4.86101 359 4.86328 336 4.86554 375 4.86781 340 4.87007 356 4.87233 338 4.8746 310 4.87686 351 4.87913 324 4.88139 345 4.88365 342 4.88592 335 4.88818 349 4.89044 361 4.89271 335 4.89497 369 4.89724 325 4.8995 330 4.90176 339 4.90403 350 4.90629 361 4.90856 340 4.91082 351 4.91308 326 4.91535 329 4.91761 348 4.91988 323 4.92214 363 4.9244 348 4.92667 317 4.92893 369 4.9312 363 4.93346 376 4.93572 426 4.93799 539 4.94025 559 4.94252 475 4.94478 388 4.94704 358 4.94931 329 4.95157 331 4.95384 333 4.9561 319 4.95836 316 4.96063 307 4.96289 339 4.96516 332 4.96742 323 4.96968 349 4.97195 333 4.97421 354 4.97648 354 4.97874 371 4.981 349 4.98327 350 4.98553 344 4.9878 331 4.99006 359 4.99232 337 4.99459 335 4.99685 345 4.99912 323 5.00138 358 5.00364 353 5.00591 375 5.00817 336 5.01044 378 5.01342 354 5.01665 354 5.01988 345 5.02311 346 5.02633 343 5.02956 347 5.03279 341 5.03601 344 5.03924 336 5.04247 325 5.0457 331 5.04892 341 5.05215 349 5.05538 332 5.05861 359 5.06183 365 5.06506 375 5.06829 366 5.07152 377 5.07474 384 5.07797 371 5.0812 360 5.08442 382 5.08765 329 5.09088 357 5.09411 377 5.09733 383 5.10056 380 5.10379 431 5.10702 440 5.11024 408 5.11347 418 5.1167 346 5.11993 328 5.12315 303 5.12638 294 5.12961 321 5.13283 288 5.13606 290 5.13929 255 5.14252 257 5.14574 401 5.14897 838 5.1522 1047 5.15543 1029 5.15865 1372 5.16188 1386 5.16511 707 5.16834 223 5.17156 102 5.17479 87 5.17802 88 5.18124 75 5.18447 98 5.1877 99 5.19093 91 5.19415 81 5.19738 70 5.20061 60 5.20384 72 5.20706 81 5.21029 75 5.21352 84 5.21675 81 5.21997 87 5.2232 82 5.22643 90 5.22965 76 5.23288 85 5.23611 95 5.23934 96 5.24256 98 5.24579 75 5.24902 79 5.25225 91 5.25547 73 5.2587 79 5.26193 81 5.26516 73 5.26838 80 5.27161 65 5.27484 69 5.27806 77 5.28129 73 5.28452 83 5.28775 66 5.29097 75 5.2942 81 5.29743 88 5.30066 81 5.30388 70 5.30711 88 5.31034 82 5.31381 79 5.31803 75 5.32226 77 5.32648 64 5.33071 84 5.33493 92 5.33916 88 5.34338 84 5.34761 84 5.35183 83 5.35606 81 5.36028 82 5.36451 79 5.36873 80 5.37296 70 5.37718 60 5.38141 88 5.38564 89 5.38986 94 5.39409 85 5.39831 82 5.40254 71 5.40676 82 5.41099 73 5.41521 94 5.41944 93 5.42366 87 5.42789 86 5.43211 89 5.43634 77 5.44056 95 5.44479 99 5.44902 86 5.45324 85 5.45747 79 5.46169 82 5.46592 101 5.47014 94 5.47437 79 5.47859 88 5.48282 78 5.48704 87 5.49127 82 5.49549 76 5.49972 73 5.50394 94 5.50817 87 5.5124 85 5.51662 77 5.52085 92 5.52507 76 5.5293 73 5.53352 63 5.53775 79 5.54197 93 5.5462 97 5.55042 106 5.55465 94 5.55887 94 5.5631 98 5.56732 84 5.57155 89 5.57578 90 5.58 97 5.58423 100 5.58845 91 5.59268 83 5.5969 107 5.60113 98 5.60535 98 5.60958 98 5.6138 86 5.61803 94 5.62225 89 5.62648 97 5.6307 103 5.63493 72 5.63916 111 5.64338 112 5.64761 107 5.65183 103 5.65606 88 5.66028 85 5.66451 96 5.66873 106 5.67296 96 5.67718 88 5.68141 95 5.68563 99 5.68986 99 5.69408 107 5.69831 98 5.70254 96 5.70676 86 5.71099 93 5.71521 97 5.71944 82 5.72366 130 5.72789 121 5.73211 138 5.73634 151 5.74056 124 5.74479 98 5.74901 91 5.75324 87 5.75746 115 5.76169 94 5.76591 81 5.77014 76 5.77437 92 5.77859 101 5.78282 81 5.78704 86 5.79127 86 5.79549 85 5.79972 73 5.80394 81 5.80817 103 5.81239 82 5.81662 79 5.82084 88 5.82507 109 5.8293 172 5.83352 246 5.83775 254 5.84197 222 5.8462 154 5.85042 82 5.85465 54 5.85887 43 5.8631 45 5.86732 39 5.87155 44 5.87577 39 5.87603 40 5.87603 57 5.87603 70 5.87603 83 5.87603 113 5.87603 76 5.87603 55 5.87603 45 5.87603 29 5.87603 17 5.87603 21 5.87603 16 5.87603 14 5.87603 19 5.87603 8 5.87603 14 5.87603 11 5.87603 33 5.87603 57 5.87603 59 5.87603 64 5.87603 49 5.87603 24 5.87603 21 5.87603 6 5.87603 1 5.87603 1 5.87603 1 5.87603 O 1s/2 pnb.vms 2015 10 14 9 41 26 0 13 Casa Info Follows 1 Calib M = 280.883 A = 284.6 BE ADD 0 1 CASA region (*O 1s*) (*Shirley*) 942.973 962.973 0.78 2 0 0 299 542 275 9.3 (*O 1s*) 15.9994 0 2 CASA comp (*O 1s*) (*GL(30)*) Area 2853.6821 0.001 10000000 -1 1 MFWHM 1.703286 0.38 9.5 -1 1 Position 956.25478 942.973 962.973 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) CASA comp (*O 1s*) (*GL(30)*) Area 253.7105 0.001 10000000 -1 1 MFWHM 1.2814813 0.37074578 9.2686445 -1 1 Position 954.4769 942.973 962.973 -1 1 RSF 0.78 MASS 15.9994 INDEX -1 (*O 1s*) CONST (**) pnb.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 666 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 332 Charge Neutraliser :On Acquired On :15/10/14 09:41:26 XPS 55 6 3 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 O 1s -1 Kinetic Energy eV 946.69 0.1 2 Intensity d Transmission d pulse counting 0.3315 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 1367 6767 1.31473 1.31659 1973 1.31659 1982 1.31658 2001 1.31657 2009 1.31656 1943 1.31655 1879 1.31654 1961 1.31653 1886 1.31652 1941 1.31651 1857 1.3165 1874 1.3165 1949 1.31649 1852 1.31648 1942 1.31647 1872 1.31646 1871 1.31645 1872 1.31644 1904 1.31643 1901 1.31642 1846 1.31641 1848 1.3164 1800 1.31639 1852 1.31638 1803 1.31637 1805 1.31637 1784 1.31636 1777 1.31635 1830 1.31634 1867 1.31633 1777 1.31632 1792 1.31631 1714 1.3163 1726 1.31629 1801 1.31628 1757 1.31627 1706 1.31626 1726 1.31625 1749 1.31624 1706 1.31623 1713 1.31623 1793 1.31622 1740 1.31621 1697 1.3162 1733 1.31619 1736 1.31618 1746 1.31617 1762 1.31616 1774 1.31615 1746 1.31614 1735 1.31613 1751 1.31612 1713 1.31611 1685 1.3161 1676 1.3161 1645 1.31609 1683 1.31608 1704 1.31607 1741 1.31606 1696 1.31605 1687 1.31604 1728 1.31603 1704 1.31602 1697 1.31601 1745 1.316 1681 1.31599 1696 1.31598 1682 1.31597 1652 1.31597 1712 1.31596 1711 1.31595 1704 1.31594 1715 1.31593 1597 1.31592 1642 1.31591 1671 1.3159 1694 1.31589 1682 1.31588 1635 1.31587 1703 1.31586 1724 1.31585 1733 1.31584 1660 1.31584 1644 1.31583 1685 1.31582 1653 1.31581 1610 1.3158 1645 1.31579 1683 1.31578 1660 1.31577 1649 1.31576 1663 1.31575 1590 1.31574 1614 1.31573 1640 1.31572 1729 1.31571 1585 1.3157 1663 1.3157 1706 1.31569 1759 1.31568 1753 1.31567 1693 1.31566 1831 1.31565 1884 1.31564 1919 1.31563 1963 1.31562 2063 1.31561 2071 1.3156 2180 1.31559 2240 1.31558 2333 1.31557 2361 1.31557 2511 1.31556 2496 1.31555 2600 1.31554 2708 1.31553 2801 1.31552 2779 1.31551 2954 1.3155 3104 1.31549 3296 1.31548 3453 1.31547 3607 1.31546 3800 1.31545 4071 1.31544 4500 1.31544 4700 1.31543 5145 1.31542 5516 1.31541 5912 1.3154 6184 1.31539 6504 1.31538 6720 1.31537 6703 1.31536 6767 1.31535 6615 1.31534 6636 1.31533 6257 1.31532 5791 1.31531 5462 1.31531 5084 1.3153 4803 1.31529 4294 1.31528 3817 1.31527 3557 1.31526 3078 1.31525 2705 1.31524 2503 1.31523 2294 1.31522 2137 1.31521 2021 1.3152 1855 1.31519 1774 1.31518 1674 1.31517 1631 1.31517 1564 1.31516 1563 1.31515 1534 1.31514 1522 1.31513 1519 1.31512 1450 1.31511 1504 1.3151 1464 1.31509 1542 1.31508 1452 1.31507 1391 1.31506 1447 1.31505 1450 1.31504 1451 1.31504 1457 1.31503 1401 1.31502 1412 1.31501 1391 1.315 1429 1.31499 1448 1.31498 1492 1.31497 1443 1.31496 1476 1.31495 1415 1.31494 1460 1.31493 1377 1.31492 1367 1.31491 1505 1.31491 1440 1.3149 1447 1.31489 1570 1.31488 1423 1.31487 1440 1.31486 1489 1.31485 1467 1.31484 1461 1.31483 1409 1.31482 1497 1.31481 1489 1.3148 1378 1.31479 1422 1.31478 1451 1.31478 1384 1.31477 1471 1.31476 1407 1.31475 1455 1.31474 1481 1.31473 Nb 3p/3 pnb.vms 2015 10 14 9 41 26 0 15 Casa Info Follows 1 Calib M = 280.883 A = 284.6 BE ADD 0 1 CASA region (*Nb 3p*) (*Shirley*) 1090.973 1134.973 2.63 2 0 0 299 542 275 9.3 (*Nb 3p*) 92.9064 0 4 CASA comp (*Nb 3p*) (*GL(30)*) Area 2105.614 0.001 10000000 -1 1 MFWHM 2.5360868 0.54 13.5 -1 1 Position 1121.1725 1090.973 1134.973 -1 1 RSF 2.63 MASS 92.9064 INDEX -1 (*Nb 3p*) CONST (**) CASA comp (*Nb 3p*) (*GL(30)*) Area 1160.3486 0.001 10000000 -1 1 MFWHM 2.4365727 0.54 13.5 -1 1 Position 1105.661 1090.973 1134.973 -1 1 RSF 2.63 MASS 92.9064 INDEX -1 (*Nb 3p*) CONST (**) CASA comp (*Nb 3p*) (*GL(30)*) Area 497.77791 0.001 10000000 -1 1 MFWHM 4.9357884 0.5667759 14.169398 -1 1 Position 1123.6633 1090.973 1134.973 -1 1 RSF 2.63 MASS 92.9064 INDEX -1 (*Nb 3p*) CONST (**) CASA comp (*Nb 3p*) (*GL(30)*) Area 253.66711 0.001 10000000 -1 1 MFWHM 3.0013612 0.68742604 17.185651 -1 1 Position 1107.8756 1090.973 1134.973 -1 1 RSF 2.63 MASS 92.9064 INDEX -1 (*Nb 3p*) CONST (**) pnb.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 2871 Sweeps: 50 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 130 Charge Neutraliser :On Acquired On :15/10/14 09:41:26 XPS 55 6 3 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Nb 3p -1 Kinetic Energy eV 1094.69 0.1 2 Intensity d Transmission d pulse counting 0.1302 50 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 882 1930 7877 1.26578 1.28386 3449 1.28386 3504 1.28381 3410 1.28377 3395 1.28373 3421 1.28369 3523 1.28365 3520 1.28361 3437 1.28357 3356 1.28353 3384 1.28349 3379 1.28344 3420 1.2834 3346 1.28336 3492 1.28332 3429 1.28328 3513 1.28324 3525 1.2832 3412 1.28316 3325 1.28312 3423 1.28307 3496 1.28303 3371 1.28299 3430 1.28295 3384 1.28291 3307 1.28287 3363 1.28283 3383 1.28279 3308 1.28275 3367 1.2827 3396 1.28266 3376 1.28262 3324 1.28258 3425 1.28254 3422 1.2825 3311 1.28246 3317 1.28242 3239 1.28238 3436 1.28234 3212 1.28229 3423 1.28225 3321 1.28221 3207 1.28217 3313 1.28213 3393 1.28209 3268 1.28205 3396 1.28201 3241 1.28197 3254 1.28192 3332 1.28188 3403 1.28184 3402 1.2818 3273 1.28176 3370 1.28172 3280 1.28168 3285 1.28164 3331 1.2816 3334 1.28155 3321 1.28151 3263 1.28147 3311 1.28143 3300 1.28139 3284 1.28135 3285 1.28131 3269 1.28127 3236 1.28123 3384 1.28118 3143 1.28114 3415 1.2811 3273 1.28106 3483 1.28102 3379 1.28098 3411 1.28094 3280 1.2809 3328 1.28086 3202 1.28082 3319 1.28077 3382 1.28073 3321 1.28069 3335 1.28065 3261 1.28061 3377 1.28057 3248 1.28053 3250 1.28049 3249 1.28045 3326 1.2804 3341 1.28036 3260 1.28032 3242 1.28028 3300 1.28024 3269 1.2802 3325 1.28016 3299 1.28012 3233 1.28008 3343 1.28003 3165 1.27999 3299 1.27995 3192 1.27991 3339 1.27987 3205 1.27983 3230 1.27979 3267 1.27975 3274 1.27971 3225 1.27966 3354 1.27962 3251 1.27958 3303 1.27954 3333 1.2795 3219 1.27946 3385 1.27942 3319 1.27938 3346 1.27934 3341 1.2793 3367 1.27925 3307 1.27921 3480 1.27917 3385 1.27913 3340 1.27909 3497 1.27905 3380 1.27901 3528 1.27897 3543 1.27893 3530 1.27888 3688 1.27884 3654 1.2788 3728 1.27876 3668 1.27872 3840 1.27868 3835 1.27864 3997 1.2786 4026 1.27856 4172 1.27851 4330 1.27847 4329 1.27843 4555 1.27839 4788 1.27835 4927 1.27831 5006 1.27827 5078 1.27823 5319 1.27819 5351 1.27814 5537 1.2781 5716 1.27806 5951 1.27802 5876 1.27798 5990 1.27794 6134 1.2779 6265 1.27786 6224 1.27782 6209 1.27778 6086 1.27773 6010 1.27769 5774 1.27765 5788 1.27761 5778 1.27757 5627 1.27753 5409 1.27749 5360 1.27745 5056 1.27741 4906 1.27736 4896 1.27732 4535 1.27728 4563 1.27724 4495 1.2772 4419 1.27716 4149 1.27712 4154 1.27708 4010 1.27704 3925 1.27699 3904 1.27695 3821 1.27691 3773 1.27687 3668 1.27683 3635 1.27679 3456 1.27675 3567 1.27671 3589 1.27667 3348 1.27662 3364 1.27658 3347 1.27654 3365 1.2765 3239 1.27646 3316 1.27642 3307 1.27638 3159 1.27634 3155 1.2763 3069 1.27626 3214 1.27621 3139 1.27617 3223 1.27613 3079 1.27609 3019 1.27605 3091 1.27601 3036 1.27597 2945 1.27593 3056 1.27589 2883 1.27584 3094 1.2758 2944 1.27576 2951 1.27572 2915 1.27568 2893 1.27564 2942 1.2756 2855 1.27556 2827 1.27552 2907 1.27547 2890 1.27543 3055 1.27539 2829 1.27535 2840 1.27531 2809 1.27527 2826 1.27523 2805 1.27519 2820 1.27515 2843 1.2751 2789 1.27506 2792 1.27502 2852 1.27498 2820 1.27494 2800 1.2749 2812 1.27486 2789 1.27482 2817 1.27478 2867 1.27474 2780 1.27469 2875 1.27465 2792 1.27461 2852 1.27457 2909 1.27453 2842 1.27449 2667 1.27445 2832 1.27441 2816 1.27437 2772 1.27432 2855 1.27428 2837 1.27424 2721 1.2742 2739 1.27416 2768 1.27412 2697 1.27408 2883 1.27404 2682 1.274 2822 1.27395 2810 1.27391 2780 1.27387 2783 1.27383 2806 1.27379 2833 1.27375 2773 1.27371 2787 1.27367 2766 1.27363 2759 1.27358 2775 1.27354 2688 1.2735 2725 1.27346 2862 1.27342 2710 1.27338 2715 1.27334 2658 1.2733 2761 1.27326 2743 1.27322 2770 1.27317 2804 1.27313 2844 1.27309 2874 1.27305 2795 1.27301 2780 1.27297 2790 1.27293 2818 1.27289 2908 1.27285 2961 1.2728 2934 1.27276 3029 1.27272 3046 1.27268 3021 1.27264 3139 1.2726 3259 1.27256 3228 1.27252 3356 1.27248 3326 1.27243 3498 1.27239 3515 1.27235 3697 1.27231 3918 1.27227 4072 1.27223 4148 1.27219 4436 1.27215 4617 1.27211 4770 1.27206 5093 1.27202 5205 1.27198 5766 1.27194 5862 1.2719 6030 1.27186 6450 1.27182 6590 1.27178 6838 1.27174 7088 1.2717 7381 1.27165 7334 1.27161 7492 1.27157 7729 1.27153 7877 1.27149 7780 1.27145 7760 1.27141 7630 1.27137 7566 1.27133 7528 1.27128 7063 1.27124 7028 1.2712 6653 1.27116 6320 1.27112 6036 1.27108 5818 1.27104 5743 1.271 5396 1.27096 5037 1.27091 4828 1.27087 4682 1.27083 4363 1.27079 4129 1.27075 4009 1.27071 3936 1.27067 3652 1.27063 3600 1.27059 3419 1.27054 3333 1.2705 3232 1.27046 3211 1.27042 3150 1.27038 2940 1.27034 2873 1.2703 2878 1.27026 2806 1.27022 2758 1.27018 2595 1.27013 2607 1.27009 2595 1.27005 2668 1.27001 2630 1.26997 2520 1.26993 2493 1.26989 2489 1.26985 2421 1.26981 2438 1.26976 2402 1.26972 2410 1.26968 2401 1.26964 2252 1.2696 2314 1.26956 2270 1.26952 2293 1.26948 2305 1.26944 2222 1.26939 2337 1.26935 2225 1.26931 2220 1.26927 2268 1.26923 2193 1.26919 2194 1.26915 2155 1.26911 2193 1.26907 2221 1.26902 2215 1.26898 2129 1.26894 2055 1.2689 2151 1.26886 2094 1.26882 2103 1.26878 2102 1.26874 2190 1.2687 2108 1.26866 2155 1.26861 2034 1.26857 2052 1.26853 2034 1.26849 2157 1.26845 2037 1.26841 2103 1.26837 2087 1.26833 2130 1.26829 2046 1.26824 2094 1.2682 2082 1.26816 2140 1.26812 2082 1.26808 2030 1.26804 2106 1.268 2104 1.26796 2018 1.26792 2064 1.26787 2094 1.26783 2064 1.26779 2081 1.26775 1935 1.26771 2020 1.26767 2080 1.26763 2023 1.26759 2065 1.26755 2045 1.2675 2078 1.26746 2133 1.26742 2109 1.26738 1977 1.26734 2035 1.2673 2015 1.26726 2042 1.26722 1964 1.26718 2149 1.26714 2083 1.26709 1997 1.26705 1961 1.26701 1989 1.26697 2048 1.26693 2042 1.26689 2021 1.26685 2094 1.26681 2021 1.26677 1954 1.26672 2017 1.26668 1985 1.26664 2021 1.2666 2099 1.26656 2040 1.26652 2016 1.26648 1990 1.26644 2028 1.2664 1986 1.26635 2025 1.26631 1930 1.26627 2019 1.26623 2037 1.26619 2056 1.26615 2055 1.26611 2012 1.26607 2004 1.26603 2122 1.26598 1973 1.26594 1997 1.2659 2078 1.26586 1981 1.26582 1948 1.26578 C 1s/4 pnb.vms 2015 10 14 9 41 26 0 14 Casa Info Follows 1 Calib M = 280.883 A = 284.6 Regions Comps BE ADD 0 1 CASA region (*C 1s*) (*Shirley*) 1186.69 1216.69 0.278 2 0 0 299 542 275 9.3 (*C 1s*) 12.011 0 3 CASA comp (*C 1s*) (*GL(30)*) Area 347.47717 0.001 10000000 -1 1 MFWHM 1.5423626 0.4 10 -1 1 Position 1205.9615 1186.69 1216.69 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) CASA comp (*C 1s*) (*GL(30)*) Area 248.63867 0.001 10000000 -1 1 MFWHM 2.2173148 0.4 10 -1 1 Position 1204.6565 1186.69 1216.69 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) CASA comp (*C 1s*) (*GL(30)*) Area 130.64411 0.001 10000000 -1 1 MFWHM 1.9567398 0.57999403 14.499851 -1 1 Position 1201.5998 1186.69 1216.69 -1 1 RSF 0.278 MASS 12.011 INDEX -1 (*C 1s*) CONST (**) pnb.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 782 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 260 Charge Neutraliser :On Acquired On :15/10/14 09:41:26 XPS 55 6 3 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 C 1s -1 Kinetic Energy eV 1186.69 0.1 2 Intensity d Transmission d pulse counting 0.2597 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 602 731 1538 1.23374 1.24606 819 1.24606 844 1.24602 845 1.24598 825 1.24594 827 1.2459 852 1.24586 915 1.24581 862 1.24577 805 1.24573 921 1.24569 897 1.24565 835 1.24561 837 1.24557 868 1.24553 839 1.24549 884 1.24544 859 1.2454 841 1.24536 836 1.24532 858 1.24528 824 1.24524 801 1.2452 824 1.24516 806 1.24512 837 1.24507 818 1.24503 827 1.24499 837 1.24495 819 1.24491 842 1.24487 829 1.24483 783 1.24479 814 1.24475 778 1.24471 864 1.24466 783 1.24462 893 1.24458 820 1.24454 836 1.2445 804 1.24446 842 1.24442 826 1.24438 845 1.24434 836 1.24429 839 1.24425 843 1.24421 868 1.24417 889 1.24413 854 1.24409 822 1.24405 811 1.24401 762 1.24397 847 1.24392 826 1.24388 879 1.24384 860 1.2438 820 1.24376 834 1.24372 853 1.24368 866 1.24364 836 1.2436 836 1.24355 823 1.24351 826 1.24347 792 1.24343 829 1.24339 822 1.24335 806 1.24331 858 1.24327 844 1.24323 881 1.24319 835 1.24314 803 1.2431 816 1.24306 844 1.24302 882 1.24298 781 1.24294 826 1.2429 832 1.24286 864 1.24282 852 1.24277 839 1.24273 810 1.24269 840 1.24265 817 1.24261 809 1.24257 824 1.24253 834 1.24249 831 1.24245 824 1.2424 841 1.24236 837 1.24232 818 1.24228 842 1.24224 829 1.2422 814 1.24216 857 1.24212 776 1.24208 812 1.24203 812 1.24199 784 1.24195 815 1.24191 814 1.24187 797 1.24183 764 1.24179 824 1.24175 777 1.24171 809 1.24167 860 1.24162 816 1.24158 830 1.24154 811 1.2415 818 1.24146 790 1.24142 825 1.24138 789 1.24134 848 1.2413 810 1.24125 854 1.24121 833 1.24117 866 1.24113 878 1.24109 846 1.24105 783 1.24101 796 1.24097 814 1.24093 817 1.24088 847 1.24084 795 1.2408 834 1.24076 839 1.24072 823 1.24068 795 1.24064 785 1.2406 880 1.24056 915 1.24051 832 1.24047 859 1.24043 933 1.24039 907 1.24035 859 1.24031 950 1.24027 943 1.24023 932 1.24019 958 1.24015 1053 1.2401 903 1.24006 929 1.24002 1005 1.23998 994 1.23994 947 1.2399 981 1.23986 977 1.23982 961 1.23978 977 1.23973 964 1.23969 937 1.23965 946 1.23961 952 1.23957 919 1.23953 941 1.23949 896 1.23945 942 1.23941 916 1.23936 949 1.23932 921 1.23928 895 1.23924 925 1.2392 952 1.23916 1021 1.23912 987 1.23908 1028 1.23904 1055 1.23899 1008 1.23895 1085 1.23891 1064 1.23887 1103 1.23883 1084 1.23879 1113 1.23875 1174 1.23871 1174 1.23867 1206 1.23863 1267 1.23858 1309 1.23854 1227 1.2385 1297 1.23846 1358 1.23842 1362 1.23838 1467 1.23834 1427 1.2383 1470 1.23826 1400 1.23821 1538 1.23817 1531 1.23813 1382 1.23809 1317 1.23805 1365 1.23801 1368 1.23797 1233 1.23793 1221 1.23789 1132 1.23784 1084 1.2378 1064 1.23776 983 1.23772 987 1.23768 946 1.23764 909 1.2376 881 1.23756 858 1.23752 845 1.23747 835 1.23743 869 1.23739 798 1.23735 792 1.23731 793 1.23727 801 1.23723 830 1.23719 784 1.23715 817 1.23711 787 1.23706 798 1.23702 817 1.23698 795 1.23694 766 1.2369 766 1.23686 818 1.23682 823 1.23678 773 1.23674 829 1.23669 805 1.23665 818 1.23661 818 1.23657 789 1.23653 805 1.23649 758 1.23645 832 1.23641 818 1.23637 825 1.23632 784 1.23628 850 1.23624 822 1.2362 820 1.23616 804 1.23612 839 1.23608 835 1.23604 794 1.236 788 1.23595 827 1.23591 837 1.23587 826 1.23583 810 1.23579 796 1.23575 814 1.23571 791 1.23567 779 1.23563 820 1.23559 893 1.23554 818 1.2355 808 1.23546 819 1.23542 854 1.23538 731 1.23534 823 1.2353 849 1.23526 775 1.23522 785 1.23517 782 1.23513 755 1.23509 807 1.23505 809 1.23501 842 1.23497 817 1.23493 834 1.23489 779 1.23485 850 1.2348 756 1.23476 795 1.23472 803 1.23468 768 1.23464 818 1.2346 849 1.23456 839 1.23452 832 1.23448 783 1.23443 780 1.23439 798 1.23435 777 1.23431 804 1.23427 788 1.23423 829 1.23419 824 1.23415 848 1.23411 786 1.23407 805 1.23402 808 1.23398 800 1.23394 786 1.2339 774 1.23386 761 1.23382 864 1.23378 822 1.23374 Nb 3d/5 pnb.vms 2015 10 14 9 41 26 0 13 Casa Info Follows 1 Calib M = 280.883 A = 284.6 BE ADD 0 1 CASA region (*Nb 3d*) (*Shirley*) 1272.973 1285.973 2.921 2 0 0 299 542 275 9.3 (*Nb 3d*) 92.9064 0 2 CASA comp (*Nb 3d*) (*GL(30)*) Area 3322.4164 0.001 10000000 -1 1 MFWHM 1.4574917 0.32 8 -1 1 Position 1279.3769 1272.973 1285.973 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) CASA comp (*Nb 3d*) (*GL(30)*) Area 2027.6563 0.001 10000000 -1 1 MFWHM 1.3680499 0.32 8 -1 1 Position 1276.6161 1272.973 1285.973 -1 1 RSF 2.921 MASS 92.9064 INDEX -1 (*Nb 3d*) CONST (**) pnb.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 1200 Sweeps: 20 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 458 Charge Neutraliser :On Acquired On :15/10/14 09:41:26 XPS 55 6 3 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Nb 3d -1 Kinetic Energy eV 1276.69 0.1 2 Intensity d Transmission d pulse counting 0.458 20 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 262 662 20435 1.20732 1.2118 2180 1.2118 2229 1.21177 2159 1.21173 2086 1.2117 2114 1.21166 2068 1.21163 2093 1.21159 1987 1.21156 1962 1.21152 1980 1.21149 1981 1.21146 1908 1.21142 1913 1.21139 1876 1.21135 1838 1.21132 1809 1.21128 1846 1.21125 1860 1.21121 1979 1.21118 1966 1.21115 2102 1.21111 2184 1.21108 2543 1.21104 2743 1.21101 3326 1.21097 3883 1.21094 4604 1.2109 5535 1.21087 6786 1.21084 7818 1.2108 9365 1.21077 10458 1.21073 11634 1.2107 12767 1.21066 13270 1.21063 13950 1.21059 14268 1.21056 13979 1.21053 13404 1.21049 13048 1.21046 11909 1.21042 11146 1.21039 10075 1.21035 8702 1.21032 7673 1.21029 6718 1.21025 5833 1.21022 5103 1.21018 4342 1.21015 4104 1.21011 4004 1.21008 4206 1.21004 4776 1.21001 5653 1.20998 6772 1.20994 8159 1.20991 9911 1.20987 11737 1.20984 13988 1.2098 15733 1.20977 17294 1.20973 18917 1.2097 19644 1.20967 20237 1.20963 20435 1.2096 19672 1.20956 18961 1.20953 17850 1.20949 16313 1.20946 14803 1.20942 13130 1.20939 11167 1.20936 9649 1.20932 7981 1.20929 6731 1.20925 5359 1.20922 4346 1.20918 3478 1.20915 2778 1.20911 2243 1.20908 1863 1.20905 1518 1.20901 1218 1.20898 1120 1.20894 996 1.20891 957 1.20887 979 1.20884 828 1.2088 860 1.20877 763 1.20874 754 1.2087 735 1.20867 817 1.20863 747 1.2086 782 1.20856 733 1.20853 736 1.20849 702 1.20846 697 1.20843 708 1.20839 705 1.20836 700 1.20832 674 1.20829 677 1.20825 721 1.20822 662 1.20819 696 1.20815 712 1.20812 705 1.20808 686 1.20805 725 1.20801 678 1.20798 701 1.20794 697 1.20791 762 1.20788 729 1.20784 725 1.20781 749 1.20777 797 1.20774 800 1.2077 732 1.20767 724 1.20763 755 1.2076 797 1.20757 772 1.20753 767 1.2075 863 1.20746 815 1.20743 763 1.20739 811 1.20736 808 1.20732 Si 2p/6 pnb.vms 2015 10 14 9 41 26 0 10 Casa Info Follows 1 Calib M = 280.883 A = 284.6 BE ADD 0 0 0 pnb.vms Dir:c:\users\tapiarem\desktop\phd\lab results\xps\xps data\niobium\ XPS Spectrum Lens Mode:Hybrid Resolution:Pass energy 40 Acqn. Time(s): 799 Sweeps: 10 Anode:Mono(Al (Mono))(156 W) Step(meV): 100.0 Dwell Time(ms): 397 Charge Neutraliser :On Acquired On :15/10/14 09:41:26 XPS 55 6 3 Mono(Al (Mono)) 1486.69 156 1e+037 1e+037 3000 3000 1e+037 1e+037 FAT 40 1e+037 -5.17 0 1e+037 1e+037 1e+037 1e+037 Si 2p -1 Kinetic Energy eV 1376.69 0.1 2 Intensity d Transmission d pulse counting 0.3974 10 0 1e+037 1e+037 1e+037 1 MFP Exponent d 0 402 285 405 1.19156 1.19218 358 1.19218 312 1.19218 329 1.19217 300 1.19217 314 1.19217 316 1.19216 341 1.19216 288 1.19216 324 1.19215 297 1.19215 320 1.19215 339 1.19214 325 1.19214 345 1.19214 314 1.19213 318 1.19213 308 1.19213 329 1.19213 316 1.19212 298 1.19212 332 1.19212 321 1.19211 308 1.19211 320 1.19211 329 1.1921 331 1.1921 311 1.1921 347 1.19209 291 1.19209 311 1.19209 324 1.19209 317 1.19208 347 1.19208 332 1.19208 286 1.19207 298 1.19207 352 1.19207 301 1.19206 311 1.19206 338 1.19206 337 1.19205 305 1.19205 336 1.19205 353 1.19205 285 1.19204 336 1.19204 304 1.19204 314 1.19203 344 1.19203 318 1.19203 314 1.19202 345 1.19202 334 1.19202 315 1.19201 299 1.19201 324 1.19201 301 1.19201 309 1.192 335 1.192 297 1.192 352 1.19199 295 1.19199 310 1.19199 302 1.19198 322 1.19198 332 1.19198 302 1.19197 303 1.19197 307 1.19197 294 1.19196 313 1.19196 303 1.19196 351 1.19196 315 1.19195 344 1.19195 342 1.19195 357 1.19194 359 1.19194 330 1.19194 317 1.19193 329 1.19193 295 1.19193 346 1.19192 309 1.19192 334 1.19192 331 1.19192 362 1.19191 317 1.19191 315 1.19191 355 1.1919 354 1.1919 405 1.1919 376 1.19189 335 1.19189 349 1.19189 365 1.19188 345 1.19188 330 1.19188 371 1.19188 356 1.19187 352 1.19187 340 1.19187 392 1.19186 310 1.19186 356 1.19186 356 1.19185 313 1.19185 340 1.19185 367 1.19184 320 1.19184 296 1.19184 339 1.19184 344 1.19183 355 1.19183 330 1.19183 343 1.19182 369 1.19182 345 1.19182 318 1.19181 370 1.19181 321 1.19181 348 1.1918 348 1.1918 343 1.1918 354 1.1918 334 1.19179 319 1.19179 332 1.19179 316 1.19178 352 1.19178 355 1.19178 345 1.19177 330 1.19177 296 1.19177 286 1.19176 329 1.19176 312 1.19176 336 1.19176 329 1.19175 318 1.19175 374 1.19175 352 1.19174 313 1.19174 338 1.19174 374 1.19173 315 1.19173 308 1.19173 319 1.19172 323 1.19172 294 1.19172 298 1.19171 310 1.19171 350 1.19171 314 1.19171 315 1.1917 305 1.1917 316 1.1917 356 1.19169 372 1.19169 311 1.19169 354 1.19168 333 1.19168 346 1.19168 303 1.19167 335 1.19167 306 1.19167 319 1.19167 336 1.19166 352 1.19166 297 1.19166 314 1.19165 336 1.19165 312 1.19165 319 1.19164 331 1.19164 391 1.19164 342 1.19163 319 1.19163 341 1.19163 323 1.19163 347 1.19162 349 1.19162 306 1.19162 332 1.19161 350 1.19161 336 1.19161 375 1.1916 369 1.1916 345 1.1916 318 1.19159 311 1.19159 341 1.19159 316 1.19159 337 1.19158 313 1.19158 312 1.19158 335 1.19157 345 1.19157 331 1.19157 307 1.19156 352 1.19156 end of experiment